2a,3,4,5-四氢苊合成路线 (共 27 条)
反应条件
triethylsilane; 2C2H3F3O*BF3 in dichloromethane
T=20°C; 4 h;
参考文献
Prakash, G. K. Surya; Mathew, Thomas; Marinez, Eric R.; Esteves, Pierre M.; Rasul, Golam; Olah, George A.
Journal of Organic Chemistry, 2006 , vol. 71, # 10 p. 3952 - 3958
反应条件
nickel; decalin
T=230°C; Hydrogenation;
参考文献
v. Braun; Bayer
Chemische Berichte, 1926 , vol. 59, p. 922
反应条件
tetra-n-propyl-diborane; hydrogen in n-heptane
T=200°C; P=75006 Torr; 0.5 h; Product distribution;
参考文献
Yalpani, Mohamed; Lunow, Thomas; Koester, Roland
Chemische Berichte, 1989 , vol. 122, p. 687 - 694
反应条件
tetra-n-propyl-diborane; hydrogen in toluene
T=200°C; P=75006 Torr; 4 h; Product distribution;
参考文献
Yalpani, Mohamed; Lunow, Thomas; Koester, Roland
Chemische Berichte, 1989 , vol. 122, p. 687 - 694
反应条件
T=110 - 115°C; Hydrogenation;
参考文献
Johnson; Glenn
Journal of the American Chemical Society, 1949 , vol. 71, p. 1092,1095
反应条件
aluminum oxide; nickel molybdenum; hydrogen
T=390°C; P=45003.6 Torr; 0.166667 h; var. temp., var. time; Product distributionKineticsMechanism;
参考文献
Miki, Yasuo; Sugimoto, Yoshikazu
Bulletin of the Chemical Society of Japan, 1995 , vol. 68, # 3 p. 723 - 729
反应条件
perchloric acid
T=50°C; Rate constant;
参考文献
Gruber, Rene; Kirsch, Gilbert; Cagniant, Denise
Bulletin de la Societe Chimique de France, 1987 , # 3 p. 498 - 504
反应条件
perchloric acid
T=50°C; Rate constant;
参考文献
Gruber, Rene; Kirsch, Gilbert; Cagniant, Denise
Bulletin de la Societe Chimique de France, 1987 , # 3 p. 498 - 504
反应条件
T=300 - 450°C; P=22065.2 Torr;
参考文献
du Pont de Nemours and Co.
Patent: US2073973 , 1935 ;
反应条件
Behandlung der Reaktionsloesung mit Raney-Nickel und erneuter Hydrierung an Palladium/Kohle.Hydrogenation;
参考文献
Johnson; Glenn
Journal of the American Chemical Society, 1949 , vol. 71, p. 1092,1095