1-苯基-1,3-丙二醇合成路线 （共 84 条）
反应条件
1: 0.456 g / m-chloroperbenzoic acid / CH2Cl2 / 96 h / Ambient temperature
2: LiAlH4 / diethyl ether / Ambient temperature
View Scheme
参考文献
Ayer, William A.; Browne, Lois M.; Feng, Meow-Chen; Orszanska, Helena; Saeedi-Ghomi, Hossein
Canadian Journal of Chemistry, 1986 , vol. 64, p. 904 - 909
反应条件
1: sodium hydride / mineral oil; toluene / 21 h / 20 - 110 °C / |Inert atmosphere
2: sodium tetrahydroborate / methanol / 10 °C
View Scheme
参考文献
Borowiecki, Pawel; Bretner, Maria
Tetrahedron Asymmetry, 2013 , vol. 24, # 15-16 p. 925 - 936
反应条件
lithium aluminium tetrahydride; diethyl ether
参考文献
Searles et al.
Journal of Organic Chemistry, 1959 , vol. 24, p. 1770,1773
反应条件
iodine in dichloromethane
参考文献
Atkinson,P.H. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1977 , p. 230 - 238
反应条件
sodium hydroxide; zinc(II) tetrahydroborate; dihydrogen peroxide
1.) THF, 5 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Narasimhan, S.; Madhavan, S.; Prasad, K. Ganeshwar
Journal of Organic Chemistry, 1995 , vol. 60, # 16 p. 5314 - 5315
反应条件
sulfuric acid
T=25 - 30°C; Kochen des Reaktionsprodukts mit aethanol. KOH;
参考文献
Fourneau; Benoit; Firmenich
Bulletin de la Societe Chimique de France, 1930 , vol. <4> 47, p. 894,897
反应条件
sodium hydroxide; dihydrogen peroxide
Yield given. Multistep reaction;
参考文献
Pelter, Andrew; Bugden, Gina; Rosser, Richard
Tetrahedron Letters, 1985 , vol. 26, # 41 p. 5097 - 5100
反应条件
effects of solvents , reduction agents and reaction time; Product distribution;
参考文献
Dai, Li-xin; Lou, Bo-liang; Zhang, Ying-zhi; Guo, Guang-zhong
Tetrahedron Letters, 1986 , vol. 27, # 36 p. 4343 - 4346
参考文献
Pfau; Plattner
Helvetica Chimica Acta, 1932 , vol. 15, p. 1250,1265
参考文献
Saginova. L. G.; Bondarenko, O. B.; Shabarov, Yu. S.; Gazzaev, R. A.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, p. 1935 - 1939
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 10 p. 2124 - 2129
