3-苯甲酰苯并[f]香豆素合成路线 （共 8 条）
反应条件
piperidine
T=20°C; Knoevenagel condensation; 0.0833333 h;
参考文献
Sugino, Teizo; Tanaka, Koichi
Chemistry Letters, 2001 , # 2 p. 110 - 111
反应条件
CuCl2·2H2O
T=90°C; Knoevenagel cyclocondensation; 0.166667 h; Neat (no solvent);
参考文献
Singh, Okram Mukherjee; Devi, Nepram Sushuma; Devi, Laishram Ronibala; Lim, Ki Bum; Yoon, Yong Jin; Lee, Sang-Geyong
Bulletin of the Korean Chemical Society, 2011 , vol. 32, # 1 p. 175 - 178
反应条件
ammonium acetate in acetic acid
T=20°C; Cyclization; esterification;
参考文献
Raboin, Jean-Christophe; Beley, Marc; Kirsch, Gilbert
Tetrahedron Letters, 2000 , vol. 41, # 8 p. 1175 - 1177
反应条件
in 1,4-dioxane
3 h; Heating;
参考文献
Andreichikov, Yu. S.; Tokmakova, T. N.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, # 4 p. 796 - 800
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 4 p. 880 - 885
反应条件
piperidine in ethanol
2 h; Heating;
参考文献
Umeda; Imanishi; Hirai
Chemical and Pharmaceutical Bulletin, 1980 , vol. 28, # 12 p. 3507 - 3513
反应条件
1.1: titanium tetrachloride / dichloromethane / 0.25 h / 0 °C
1.2: 20 °C
2.1: piperidine / ethanol / 2 h / |Reflux
View Scheme
参考文献
Mahajan, Sumit S.; Scian, Michele; Sripathy, Smitha; Posakony, Jeff; Lao, Uyen; Loe, Taylor K.; Leko, Vid; Thalhofer, Angel; Schuler, Aaron D.; Bedalov, Antonio; Simon, Julian A.
Journal of Medicinal Chemistry, 2014 , vol. 57, # 8 p. 3283 - 3294
反应条件
in water; dimethyl sulfoxide
T=120°C; 0.5 h; analytical procedure for PIA fluorimetric determination;
参考文献
Umeda; Imanishi; Hirai
Chemical and Pharmaceutical Bulletin, 1980 , vol. 28, # 12 p. 3507 - 3513
参考文献
Le Fevre
Journal of the Chemical Society, 1934 , p. 450,453
