tetra-(n-butyl)ammonium iodide; methyl iodide 1.) DMF, electrochemical reduction: Pt electrode, 2.) 0.5 h; Yield given. Multistep reaction. Yields of byproduct given;

tetra-(n-butyl)ammonium iodide 1.) DMF, electrochemical reduction: Hg-electrode, 2.) 0.5 h; Yield given. Multistep reaction. Yields of byproduct given;

Oxonereg;; sulfuric acid in water; acetonitrile T=25°C; var. temp. and solvents; ΔH(excit.), ΔS(excit.); Rate constantKineticsThermodynamic data;

Stage #1: <a href="#" onclick="return RXDsubstances(event, this, '1644663', constants.ctx, '0')">4,4'-dichlorodiphenyl disulfide</a> <b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '1209238', constants.ctx, '0')">aluminium trichloride</a>;&nbsp;<a href="#" onclick="return RXDsubstances(event, this, '8973685', constants.ctx, '0')">zinc</a>&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '741857', constants.ctx, '0')">acetonitrile</a> <br />T=65&deg;C;&nbsp;0.5&nbsp;h;&nbsp;<br />Stage #2: <a href="#" onclick="return RXDsubstances(event, this, '471389', constants.ctx, '0')">benzoyl chloride</a> &nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '741857', constants.ctx, '0')">acetonitrile</a> <br />T=65&deg;C;&nbsp;0.166667&nbsp;h;&nbsp;<br /> &nbsp;

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '1735581', constants.ctx, '0')">di-tert-butyl peroxide</a>&nbsp;<b>in</b>&nbsp; neat (no solvent)<br />T=120&deg;C;&nbsp;12&nbsp;h;&nbsp;&nbsp;Inert atmosphereSchlenk technique;&nbsp;<br /> &nbsp;

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '1098280', constants.ctx, '0')">tert.-butylhydroperoxide</a>;&nbsp;<a href="#" onclick="return RXDsubstances(event, this, '8128162', constants.ctx, '0')">FeBr₂</a>&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '3587155', constants.ctx, '0')">water</a> <br />T=100&deg;C;&nbsp;12&nbsp;h;&nbsp;&nbsp;Sealed tube;&nbsp;<br /> <br /> &nbsp;

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '605283', constants.ctx, '0')">triethylamine</a>;&nbsp;<a href="#" onclick="return RXDsubstances(event, this, '610776', constants.ctx, '0')">triphenylphosphine</a>;&nbsp;<a href="#" onclick="return RXDsubstances(event, this, '11324644', constants.ctx, '0')">palladium diacetate</a> <br />T=100&deg;C;&nbsp;P=10343.2&nbsp;Torr;&nbsp;18&nbsp;h;&nbsp;<br /> &nbsp;

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '28014093', constants.ctx, '0')">2-methoxycarbonyl-4,5-dichloropyridazin-3(2H)-one</a>&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '635760', constants.ctx, '0')">toluene</a> <br />4&nbsp;h;&nbsp;&nbsp;Reflux;&nbsp;<br /> &nbsp;

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '1735581', constants.ctx, '0')">di-tert-butyl peroxide</a>&nbsp;<b>in</b>&nbsp; neat (no solvent)<br />T=120&deg;C;&nbsp;24&nbsp;h;&nbsp;&nbsp;Sealed tube;&nbsp;<br /> &nbsp;

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '3902804', constants.ctx, '0')">silica gel</a> <br />T=20&deg;C;&nbsp;2.5&nbsp;h;&nbsp;<br /> &nbsp;