2,3-二溴-1-丙烯合成路线 （共 153 条）
反应条件
silver fluoride in diethylene glycol dimethyl ether
T=35 - 37°C; 120 h;
参考文献
Chen, Li-Fo; Mohtasham, Javid; Gard, Gary L.
Journal of Fluorine Chemistry, 1990 , vol. 48, # 1 p. 107 - 122
反应条件
in diethyl ether
T=0 - 20°C;
参考文献
Halasa, Adel Farhan; Hsu, Wen-Liang
Patent: US2004/63884 A1, 2004 ;
Location in patent: Page 12 ;
反应条件
tin; hydrogen bromide in diethyl ether; water
参考文献
Greenaway, Rebecca L.; Campbell, Craig D.; Chapman, Helen A.; Anderson, Edward A.
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 17 p. 3187 - 3194
反应条件
tin; hydrogen bromide in diethyl ether; water
4 h; Ambient temperature;
参考文献
Mandai, Tadakatsu; Nokami, Junzo; Yano, Toru; Yoshinaga, Yukari; Otera, Junzo
Journal of Organic Chemistry, 1984 , vol. 49, # 1 p. 172 - 174
反应条件
1: CH(CH2CH=CH2)(CO2Me)2 With sodium in methanol
0.166667 h;
2: 1,2-dibromo-2-propene in methanol
T=20°C; 20 h; Further stages.;
参考文献
Bowman, W. Russell; Krintel, Sussie L.; Schilling, Mark B.
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 4 p. 585 - 592
反应条件
1: (+/-)-2,2-dimethyl-5-phenyl-1,3-dioxolan-4-one With n-butyllithium; diisopropylamine in tetrahydrofuran; hexane
T=-78°C; 0.5 h;
2: 1,2-dibromo-2-propene in tetrahydrofuran; hexane
T=-78 - 20°C; 4 h;
参考文献
Blay, Gonzalo; Fernandez, Isabel; Monje, Belen; Pedro, Jose R.
Molecules, 2004 , vol. 9, # 5 p. 365 - 372
反应条件
tin; hydrogen bromide in diethyl ether
T=20°C;
参考文献
Beruben, Dov; Marek, Ilane; Normant, Jean F.; Platzer, Nicole
Journal of Organic Chemistry, 1995 , vol. 60, # 8 p. 2488 - 2501
反应条件
1.)in ether, 2.)in HMPA; Yield given. Multistep reaction;
参考文献
Grootaert, Werner M.; Mijngheer, Roelant; De Clercq, Pierre J.
Tetrahedron Letters, 1982 , vol. 23, # 32 p. 3287 - 3290
反应条件
copper(l) chloride in tetrahydrofuran
T=20°C; 5 h;
参考文献
Smith, Sean M.; Hoang, Gia L.; Pal, Rhitankar; Khaled, Mohammad O. Bani; Pelter, Liberty S. W.; Zeng, Xiao Cheng; Takacs, James M.
Chemical Communications, 2012 , vol. 48, # 100 p. 12180 - 12182
反应条件
sodium hydride in tetrahydrofuran
1 h; Heating;
参考文献
Bhat, Laxminarayan; Steinig, Arno G.; Appelbe, Ruth; De Meijere, Armin
European Journal of Organic Chemistry, 2001 , # 9 p. 1673 - 1680
