2,3-二甲基-1,3-丁二烯合成路线 （共 777 条）
反应条件
in benzene-d6
freeying, evacuating, heating (70°C, 3.5 h), heating (80°C, 20); chromatography (SiO2, hexane);
参考文献
Matsumoto, Tsuyoshi; Tokitoh, Norihiro; Okazaki, Renji
Journal of the American Chemical Society, 1999 , vol. 121, # 38 p. 8811 - 8824
反应条件
ozone in methanol
T=-78°C; var. solvents; Product distributionMechanism;
参考文献
Griesbaum, Karl; Zwick, Garhard; Agarwal, Sudhir; Keul, Helmut; Pfeffer, Bernd; Murray, Robert W.
Journal of Organic Chemistry, 1985 , vol. 50, # 22 p. 4194 - 4199
参考文献
Courtot
Bulletin de la Societe Chimique de France, 1906 , vol. <3>35, p. 970,971,972
反应条件
in 1-methyl-pyrrolidin-2-one
T=190°C; Diels-Alder Cycloaddition;
参考文献
Bouillon, Jean-Philippe; Mykhaylychenko, Sergiy; Melissen, Sigismund; Martinez, Agathe; Harakat, Dominique; Shermolovich, Yuriy G.
Tetrahedron, 2012 , vol. 68, # 41 p. 8663 - 8669
反应条件
in 1-methyl-pyrrolidin-2-one
T=190°C; Diels-Alder Cycloaddition; 40 h;
参考文献
Bouillon, Jean-Philippe; Mykhaylychenko, Sergiy; Melissen, Sigismund; Martinez, Agathe; Harakat, Dominique; Shermolovich, Yuriy G.
Tetrahedron, 2012 , vol. 68, # 41 p. 8663 - 8669
反应条件
in 1-methyl-pyrrolidin-2-one
T=190°C; Diels-Alder Cycloaddition;
参考文献
Bouillon, Jean-Philippe; Mykhaylychenko, Sergiy; Melissen, Sigismund; Martinez, Agathe; Harakat, Dominique; Shermolovich, Yuriy G.
Tetrahedron, 2012 , vol. 68, # 41 p. 8663 - 8669
反应条件
toluene-4-sulfonic acid in benzene
8 h; Heating;
参考文献
Alonso-Silva, Ignacio J.; Pardo, Mercedes; Soto, Jose L.
Heterocycles, 1988 , vol. 27, # 2 p. 357 - 364
