[1,1′-二环戊基]-1,1'-二醇合成路线 （共 38 条）
反应条件
Pr
1.) THF, 20 deg C, 2.) -20 deg C;
参考文献
Gailyunas, G. A.; Biktimirov, R. Kh.; Monakov, Yu. B.; Tolstikov, G. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1985 , vol. 34, p. 2629
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1985 , # 12 p. 2830 - 2831
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; samarium diiodide; methyl 3-bromo-propionate in tetrahydrofuran
Ambient temperature;
参考文献
Csuk; Hu; Abdou; Kratky
Tetrahedron, 1991 , vol. 47, # 34 p. 7037 - 7044
反应条件
Pr
1.) THF, 20 deg C, 2.) -20 deg C;
参考文献
Gailyunas, G. A.; Biktimirov, R. Kh.; Monakov, Yu. B.; Tolstikov, G. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1985 , vol. 34, p. 2629
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1985 , # 12 p. 2830 - 2831
反应条件
hydrogen; palladium on activated charcoal
参考文献
Chirko,A.I.
Journal of Organic Chemistry USSR (English Translation), 1966 , vol. 1, p. 2023 - 2025
Zhurnal Organicheskoi Khimii, 1966 , vol. 1, p. 1984 - 1987
反应条件
1: O2
2: H2 / Pd-C
View Scheme
参考文献
Chirko,A.I.
Journal of Organic Chemistry USSR (English Translation), 1966 , vol. 1, p. 2023 - 2025
Zhurnal Organicheskoi Khimii, 1966 , vol. 1, p. 1984 - 1987
反应条件
water; lithium; 4,4'-di-tert-butylbiphenyl
1.) THF, -40 deg C, 55 min; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Guijarro, Albert; Vus, Miguel
Tetrahedron Letters, 1994 , vol. 35, # 2 p. 253 - 256
反应条件
1: Ba(OH)2 / 290 - 295 °C
2: durch Reduktion
View Scheme
参考文献
Harries; Wagner
Justus Liebigs Annalen der Chemie, 1915 , vol. 410, p. 39
反应条件
aluminium
Title compound not separated from byproducts;
参考文献
Sands
Journal of Organic Chemistry, 1994 , vol. 59, # 2 p. 468 - 471
反应条件
aluminium
Title compound not separated from byproducts;
参考文献
Sands
Journal of Organic Chemistry, 1994 , vol. 59, # 2 p. 468 - 471
反应条件
titanium tetrachloride; magnesium; ethylene dibromide
1.) benzene, 0 deg C, 30 min, 2.) 5-10 deg C, 2 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Rao, S. Achyutha; Periasamy, M.
Tetrahedron Letters, 1988 , vol. 29, # 13 p. 1583 - 1586
