alpha-(三氯甲基)-4-氯苯甲醇合成路线 （共 32 条）
反应条件
1: 89.3 percent / H2SO4 / 72 h / 20 °C
2: 81.6 percent / 50percent NaOH, TEBA / diethyl ether / 2 h / 40 - 45 °C
View Scheme
参考文献
Volkov, Yu. P.; Yanovskaya, L. A.; Kryshtal', G. V.; Kalinevich, V. M.; Trusova, E. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1986 , vol. 35, # 6 p. 1242 - 1245
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1986 , # 6 p. 1368 - 1372
参考文献
Hamada; Ohno
Bl. Inst. Insect Control KyotoChem.Abstr., 1949 , vol. 13, p. 19
Bl. Inst. Insect Control KyotoChem.Abstr., 1950 , p. 2960
反应条件
phosphorus pentachloride
参考文献
Zasorina,V.A. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1979 , vol. 49, # 6 p. 1222 - 1225,1072 - 1074
反应条件
potassium hydroxide in ethylene glycol
参考文献
Reeve,W.; Barron,E.R.
Journal of Organic Chemistry, 1975 , vol. 40, p. 1917 - 1920
参考文献
Reeve, Wilkins; McKee, James R.; Brown, Robert; Lakshmanan, Sitarama; McKee, Gertrude A.
Canadian Journal of Chemistry, 1980 , vol. 58, p. 485 - 493
参考文献
Howard
Journal of the American Chemical Society, 1935 , vol. 57, p. 2317
参考文献
Schneller; Smith
Journal of the American Chemical Society, 1948 , vol. 70, p. 4057
反应条件
sulfuric acid; acetic anhydride
参考文献
Ettel; Weichet
Collection of Czechoslovak Chemical Communications, 1950 , vol. 15, p. 520,523
参考文献
University of Illinois Foundation
Patent: US3966824 A1, 1976 ;
反应条件
samarium diiodide in tetrahydrofuran
T=20°C; 0.0833333 h;
参考文献
Li, Jian; Xu, Xiaoliang; Zhang, Yongmin
Tetrahedron Letters, 2003 , vol. 44, # 52 p. 9349 - 9351
