P-3-吡啶基-膦酸二乙酯合成路线 （共 5 条）
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate; triethylamine in acetonitrile
modified Hirao coupling reaction; 22 h; Heating;
参考文献
Belabassi, Yamina; Alzghari, Saeed; Montchamp, Jean-Luc
Journal of Organometallic Chemistry, 2008 , vol. 693, # 19 p. 3171 - 3178
反应条件
N-ethyl-N,N-diisopropylamine; tetrakis(triphenylphosphine) palladium(0) in acetonitrile
T=70°C; 4 h; in sealed tube;
参考文献
Petrakis, Konstantinos S.; Nagabhushan, Tattanahalli L.
Journal of the American Chemical Society, 1987 , vol. 109, # 9 p. 2831 - 2833
反应条件
sodium hydride in tetrahydrofuran; acetonitrile
T=25°C; 7 h; Irradiation;
参考文献
Bulot, J. J.; Aboujaoude, E. Elia; Collignon, N.; Savignac, P.
Phosphorus and Sulfur and the Related Elements, 1984 , vol. 21, p. 197 - 204
反应条件
1: 50 percent / NaNO2, KI
2: 70 percent / NaH / tetrahydrofuran; acetonitrile / 7 h / 25 °C / Irradiation
View Scheme
参考文献
Bulot, J. J.; Aboujaoude, E. Elia; Collignon, N.; Savignac, P.
Phosphorus and Sulfur and the Related Elements, 1984 , vol. 21, p. 197 - 204
反应条件
hydrogenchloride in water
12 h; Heating;
参考文献
Bulot, J. J.; Aboujaoude, E. Elia; Collignon, N.; Savignac, P.
Phosphorus and Sulfur and the Related Elements, 1984 , vol. 21, p. 197 - 204
