2-(苯基亚甲基)茚-1,3-二酮合成路线 (共 37 条)
反应条件
3,4,5,6-tetrachloro-1,2-benzoquinone
T=100°C; 8 h; Inert atmosphere;
参考文献
Li, Zhiping; Li, Haijun; Guo, Xingwei; Cao, Lin; Yu, Rong; Li, Huanrong; Pan, Shiguang
Organic Letters, 2008 , vol. 10, # 5 p. 803 - 805
反应条件
3,4,5,6-tetrachloro-1,2-benzoquinone
T=100°C; 8 h; Inert atmosphere;
参考文献
Li, Zhiping; Li, Haijun; Guo, Xingwei; Cao, Lin; Yu, Rong; Li, Huanrong; Pan, Shiguang
Organic Letters, 2008 , vol. 10, # 5 p. 803 - 805
反应条件
pyrrolidine in methanol
T=70°C; Michael/retro-Michael/Diels-Alder reaction; 5 h;
参考文献
Ramachary; Anebouselvy; Chowdari, Naidu S.; Barbas III, Carlos F.
Journal of Organic Chemistry, 2004 , vol. 69, # 18 p. 5838 - 5849
参考文献
Cubist Pharmaceuticals, Inc.
Patent: US6153645 A1, 2000 ;
反应条件
in ethanol
3 h; Heating;
参考文献
Afsah; Etman; Hamama; Sayed-Ahmed
Bollettino Chimico Farmaceutico, 1998 , vol. 137, # 7 p. 244 - 248
反应条件
in chloroform
T=-5°C;
参考文献
Magdesieva, N. N.; Sergeeva, T. A.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, # 7 p. 1454 - 1455
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 7 p. 1598 - 1599
反应条件
in hydrogenchloride; dimethyl sulfoxide
T=20°C; various pH; Rate constantEquilibrium constant;
参考文献
Bernasconi, Claude F.; Laibelman, Alan; Zitomer, Janie L.
Journal of the American Chemical Society, 1985 , vol. 107, # 23 p. 6570 - 6575
反应条件
hydrogenchloride in ethanol
2 h; Heating;
参考文献
Lusis, V. K.; Mutsenietse, D. Kh.; Dubur, G. Ya.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1986 , vol. 22, # 10 p. 1104 - 1107
Khimiya Geterotsiklicheskikh Soedinenii, 1986 , vol. 22, # 10 p. 1363 - 1366
反应条件
1: 2-benzyl-1,3-indanedione With potassium hydride in acetonitrile
T=20°C; 0.333333 h; Inert atmosphereGlovebox;
2: 4-acetylamino-2,2,6,6-tetramethylpiperidine-1-oxoammonium in acetonitrile
T=24.84°C; Inert atmosphereGlovebox; Thermodynamic data;
参考文献
Cao, Ying; Zhang, Song-Chen; Zhang, Min; Shen, Guang-Bin; Zhu, Xiao-Qing
Journal of Organic Chemistry, 2013 , vol. 78, # 14 p. 7154 - 7168
参考文献
Radulescu; Georgescu
Bulletin de la Societe Chimique de France, 1925 , vol. <4> 37, p. 1069,1187
Full Text Show Details
Ionescu
Buletinul Societatii de Stiinte din Cluj, vol. 3, p. 33
Chem. Zentralbl., 1927 , vol. 98, # I p. 601