54509-73-8合成路线 (共 3623 条)
反应条件
Ph3P(+)CH3I(-); triphenylphosphine; Rhodium trichloride in various solvent(s) T=180°C; P=60004.8 Torr; 4 h; further ereaction conditions and promotors; Product distribution;
参考文献
Tetrahedron Letters, , vol. 32, # 32 p. 3989 - 3992
反应条件
dodecacarbonyltetrarhodium(0); triphenylphosphine; isopropyl alcohol T=220°C; 5 h;
参考文献
Journal of Organometallic Chemistry, , vol. 412, # 1.2 p. 291 - 300
反应条件
dicobalt octacarbonyl; water; 1,2-bis-(diphenylphosphino)ethane in 1,4-dioxane T=165°C;
参考文献
Murata, Kazuhisa; Matsuda, Akio
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 7 p. 2089 - 2092
反应条件
hydrogen; Pt(H)(Ph2PO)(Ph2POH)2 in benzene T=100°C; P=22501.8 Torr; 7 h; Yield given. Yields of byproduct given;
参考文献
Leeuwen, Piet W. N. M. van; Roobeek, Cornelis F.; Wife, Richard L.; Frijns, John H. G.
Journal of the Chemical Society, Chemical Communications, 1986 , # 1 p. 31 - 33
反应条件
hydrogen; rhodium contaminated with carbon T=139.9°C; 8 h; other temperatures, other supported Rh catalysts; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Takahashi, Nobuo; Arakawa, Hironori; Kano, Atsuhiko; Fukagawa, Yoshimi; Asao, Kiyoyuki
Chemistry Letters, 1990 , # 2 p. 205 - 208
反应条件
water; hydrogen iodide; acetic acid; palladium diacetate in o-xylene T=170°C; 2 h; other catalysts; Product distribution;
参考文献
Lapidus, A. L.; Pirozhkov, S. D.; Vellekov, A.; Garanin, V. I.; Slyunyaev, P. I.; Minachev, Kh. M.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1983 , vol. 32, # 1 p. 119 - 124
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1983 , # 1 p. 142 - 147
反应条件
Et2PCH(Me)C(O)Me; [rhodium(I)(carbonyl)2(acetylacetonate)] T=110°C; P=52505.3 Torr; 24 h; Product distribution; Further Variations:Reagents;
参考文献
Robertson; Poole; Payne; Cole-Hamilton
Chemical Communications, 2001 , # 1 p. 47 - 48
反应条件
carbon monoxide; hydrogen; lt;Ru2(CO)4(μ-O2CEt)2(PPh2Et)2gt; in tetrahydrofuran; water T=160°C; 18 h; in the autoclave;
参考文献
Beguin, Alain; Boettcher, Hans-Christian; Suess-Fink, Georg; Walther, Bernhard
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1992 , # 13 p. 2133 - 2134
反应条件
hydrogen sulfide; hydrogen; NiMo/C T=290°C; P=7500.6 Torr; various temp. and catalysts; Product distribution;
参考文献
Vit, Zdenek; Portefaix, Jean Louis; Breysse, Michele
Collection of Czechoslovak Chemical Communications, 1997 , vol. 62, # 7 p. 1015 - 1022
反应条件
dodecacarbonyltetrarhodium(0) in acetone T=150°C; P=44130.5 Torr; variation of reaction temperature, catalyst and partial pressure of CO, ethylene and H2; Product distribution;
参考文献
Journal of Organometallic Chemistry, , vol. 334, p. 129 - 140