1: in toluene T=50°C; P=600.06 Torr; 0.333333 h; microwave irradiation; 2: With ammonium chloride in toluene 3: With water Further stages. Title compound not separated from byproducts.;
参考文献
Almansa, Raquel; Guijarro, David; Yus, Miguel
Tetrahedron Asymmetry, 2008 , vol. 19, # 11 p. 1376 - 1380
1: diethylzinc With methylmagnesium bromide in tetrahydrofuran T=20°C; 2: (RS,E)-N-benzylidene-2-methylpropane-2-sulfinamide in tetrahydrofuran T=-78°C; 1 h; 3: With hydrogenchloride in methanol Further stages. Title compound not separated from byproducts.;
参考文献
Almansa, Raquel; Guijarro, David; Yus, Miguel
Tetrahedron Asymmetry, 2008 , vol. 19, # 5 p. 603 - 606
1: diethylzinc With (3R,4S)-2,5-dimethyl-4-(pyrrolidin-1-yl)hexane-3-thiol in toluene T=20°C; 0.333333 h; 2: cyclohexanecarbaldehyde in toluene T=-20°C; 12 h; Title compound not separated from byproducts;
