2,3-二甲基-2-丁烯合成路线 (共 833 条)
反应条件
ozone
T=-254.16 - -238.16°C; 19 h; IrradiationInert atmosphere;
参考文献
Coleman, Bridgett E.; Ault, Bruce S.
Journal of Physical Chemistry A, 2010 , vol. 114, # 48 p. 12667 - 12674
反应条件
hydrogenchloride in tetrahydrofuran; diethyl ether
byproducts: H2; 2,3-dimethyl-2-butene added to a soln. of BH3*(CH3)2S in THF maintaining the temp. below 10°C; stirred for 1 h at 25°C; treated with an ethereal soln. of HCl at 0-5°C;
参考文献
Zweifel, George; Pearson, Norman R.
Journal of the American Chemical Society, 1980 , vol. 102, # 18 p. 5919 - 5920
反应条件
in tetrahydrofuran
0°C;
参考文献
Zweifel, G.
J. Organometal. Chem. 9, 1967 , vol. 9, p. 215 - 221
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Gmelin Handbook: B: B-Verb.9, 1.4.3.3, page 41 - 44
反应条件
T=350°C; P=129287 Torr;
参考文献
Cywinski,N.F.
Journal of Organic Chemistry, 1965 , vol. 30, p. 361 - 364
反应条件
T=350°C; P=129287 Torr;
参考文献
Cywinski,N.F.
Journal of Organic Chemistry, 1965 , vol. 30, p. 361 - 364
反应条件
in benzene
Irradiation;
参考文献
Verheijdt, Paul L.; Cerfontain, Hans
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1983 , # 9 p. 1343 - 1349
反应条件
in benzene
Ambient temperatureIrradiationother solvents: CH3CN or n-C6H14; KineticsQuantum yieldProduct distribution;
参考文献
Turro, Nicholas J.; Shima, Kennosuke; Chung, Chao-Jen; Tanielian, Charles; Kanfer, Sheldon
Tetrahedron Letters, 1980 , vol. 21, p. 2775 - 2778
反应条件
in benzene
Irradiation;
参考文献
Verheijdt, Paul L.; Cerfontain, Hans
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1983 , # 9 p. 1343 - 1349
反应条件
in benzene
Ambient temperatureIrradiationother solvents: CH3CN or n-C6H14; KineticsQuantum yieldProduct distribution;
参考文献
Turro, Nicholas J.; Shima, Kennosuke; Chung, Chao-Jen; Tanielian, Charles; Kanfer, Sheldon
Tetrahedron Letters, 1980 , vol. 21, p. 2775 - 2778
反应条件
methyltrioxorhenium (VII)
T=50 - 60°C; 72 h;
参考文献
Zhu, Zuolin; Espenson, James H.
Journal of the American Chemical Society, 1996 , vol. 118, # 41 p. 9901 - 9907