in dimethyl sulfoxide
T=35 - 40°C; 16 h; Irradiation;
参考文献
Russell, Glen A.; Ngoviwatchai, Preecha; Tashtoush, Hasan I.; Pla-Dalmau, Anna; Khanna, Rajive K.
Journal of the American Chemical Society, 1988 , vol. 110, # 11 p. 3530 - 3538
diphenylditellane in dimethyl sulfoxide
byproducts: PhTeHgCl; Irradiation (UV/VIS); nitrogen atmosphere; mercurial and PhTeTePh in deoxygenated solvent irradiated (275-W sunlamp, 35-40 °C, 16h);; reaction mixt. poured into water; extn. (benzene); ext. washed (water), dried (Na2SO4), concd.; C-C6H11SPh analysed by (1)H NMR, GLC and GCMS; yield detd. by (1)H NMR;;
参考文献
Russell, Glen A.; Ngoviwatchai, Preecha; Tashtoush, Hasan I.; Pla-Dalmau, Anna; Khanna, Rajive K.
Journal of the American Chemical Society, 1988 , vol. 110, # 11 p. 3530 - 3538