1,4-二氢-1,4-环氧萘合成路线 （共 84 条）
反应条件
triethylamine in diethyl ether Ambient temperature;
参考文献
Fisera, L'ubor; Pavlovic, Dusan
Collection of Czechoslovak Chemical Communications, 1984 , vol. 49, # 9 p. 1990 - 2000
反应条件
Ni(Br)2(dppe); zinc in acetonitrile T=80°C; 12 h;
参考文献
Rayabarapu, Dinesh K.; Sambaiah, Thota; Cheng, Chien-Hong
Angewandte Chemie - International Edition, 2001 , vol. 40, # 7 p. 1286 - 1288
反应条件
1: 70 percent / NaHCO3 / toluene / 36 h / 145 °C 2: 91 percent / conc. HCl / methanol / 15 h / Heating 3: 81 percent / MCPBA / CHCl3 / Ambient temperature 4: 1.) CuI / 1.) Et2O, -10 deg C, 20 min, 2.) Et2O, 0 deg C, 1 h 5: 68 percent / o-chloranil / toluene / Heating View Scheme
参考文献
Dehaen, Wim; Corens, David; L'Abbe, Gerrit
Synthesis, 1996 , # 2 p. 201 - 203
反应条件
C33H35BrNOPPd; water; caesium carbonate in methanol T=60°C; 12 h; Inert atmosphere;
参考文献
Zhang, Ting-Ke; Mo, Dong-Liang; Dai, Li-Xin; Hou, Xue-Long
Organic Letters, 2008 , vol. 10, # 23 p. 5337 - 5340
反应条件
C33H35BrNOPPd; water; caesium carbonate in methanol T=60°C; 4 h; Inert atmosphere; optical yield given as percent eeenantioselective reaction;
参考文献
Organic Letters, , vol. 10, # 23 p. 5337 - 5340
反应条件
[PdCl(C6H4CH(CH3)N(CH3)2)(P(C6H5)3)]; triethylamine 4 h; Inert atmosphere; optical yield given as percent eeenantioselective reaction;
参考文献
Organic Letters, , vol. 10, # 23 p. 5337 - 5340
参考文献
Wittig; Pohmer
Chemische Berichte, 1956 , vol. 89, p. 1334,1348
反应条件
1: With gallium; iodobenzene; aluminium T=120°C; 20 h; Inert atmosphere; 2: 1,4-dihydro-1,4-epoxynaphthalene in toluene T=0°C; 2 h;
参考文献
Tang, Xiaoping; Rawson, Daniel; Woodward, Simon
Synlett, 2010 , # 4 art. no. D32709ST, p. 636 - 638
反应条件
methylmagnesium bromide in tetrahydrofuran; diethyl ether T=45°C; 18 h;
参考文献
Tetrahedron Letters, , vol. 38, # 27 p. 4761 - 4764
反应条件
2,2'-bis-(diphenylphosphino)-1,1'- binaphthyl; silver nitrate; [RhCl(η2:η2-cycloocta-1,5-diene)]2 in 1,2-dichloro-ethane T=60°C; 8 h;
参考文献
Journal of Organic Chemistry, , vol. 72, # 21 p. 7849 - 7857
