4,4-二甲基-2-戊酮合成路线 (共 111 条)
反应条件
1: diethyl ether 2: Raney nickel / 200 °C / 110326 Torr / Hydrogenation View Scheme
参考文献
Moersch; Whitmore
Journal of the American Chemical Society, 1949 , vol. 71, p. 820
反应条件
oxygen; H5PV2Mo10O40(1,11) in acetonitrile T=60°C; P=750.06 Torr; 24 h;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 13 p. 825 - 826
参考文献
McCubbin; Adkins
Journal of the American Chemical Society, 1930 , vol. 52, p. 2549
参考文献
Courtot
Bulletin de la Societe Chimique de France, 1906 , vol. <3>35, p. 984
Full Text Show Details
Blaise; Courtot
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1905 , vol. 140, p. 371
反应条件
1: sodium; benzene 2: H2SO4 <100 percent > / bei der Destillation View Scheme
参考文献
Whitmore; Homeyer
Journal of the American Chemical Society, 1933 , vol. 55, p. 4195,4558
反应条件
ammonium chloride T=60°C; 10 h; Title compound not separated from byproducts;
参考文献
Ma, Zhenkun; Huang, Qingtao; Bobbitt, James M.
Journal of Organic Chemistry, 1993 , vol. 58, # 18 p. 4837 - 4843
反应条件
1: NaOBr 2: SOCl2 View Scheme
参考文献
Homeyer; Whitmore; Wallingford
Journal of the American Chemical Society, 1933 , vol. 55, p. 4209,4212
反应条件
lithium aluminium tetrahydride; 2,5-di-C-benzyl-1,3:4,6-di-O-benzylidene-D-mannitol in diethyl ether 2 h; Heating;
参考文献
Baggett, Neil; Simmonds, Richard J.; Stribblehill, Peter
Carbohydrate Research, 1987 , vol. 162, p. 153 - 158
参考文献
Whitmore; Homeyer
Journal of the American Chemical Society, 1933 , vol. 55, p. 4195,4558
参考文献
Whitmore et al.
Journal of the American Chemical Society, 1938 , vol. 60, p. 2462,2791