4,4-二甲基-2-戊酮合成路线 (共 111 条)
参考文献
Whitmore; Homeyer
Journal of the American Chemical Society, 1933 , vol. 55, p. 4195,4558
反应条件
1: sodium borate; diethyl ether 3: potassium acetate; acetic acid anhydride; acetic acid View Scheme
参考文献
Whitmore; Homeyer
Journal of the American Chemical Society, 1933 , vol. 55, p. 4195,4558
反应条件
water; hydrogen bromide; bromine
参考文献
Thorpe,J.W.; Warkentin,J.
Canadian Journal of Chemistry, 1973 , vol. 51, p. 927 - 935
参考文献
Beckwith,A.L.J. et al.
Australian Journal of Chemistry, 1974 , vol. 27, p. 1693 - 1710
反应条件
1: NaOBr 2: SOCl2 View Scheme
参考文献
Howard et al.
Journal of Research of the National Bureau of Standards (United States), 1947 , vol. 38, p. 391
Chem. Zentralbl., 1947 , vol. 118, p. 5291
反应条件
oxygen; H5PV2Mo10O40(1,11) in acetonitrile T=60°C; P=750.06 Torr; 24 h;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 13 p. 825 - 826
参考文献
Mallinckrodt Chem. Works.
Patent: US2004066 , 1933 ;
Full Text Show Details
Homeyer; Whitmore; Wallingford
Journal of the American Chemical Society, 1933 , vol. 55, p. 4209,4212
反应条件
(i) SeO2, dioxane, H2O, (ii) Br2, aq. NaOAc; Multistep reaction;
参考文献
Fischer,G. et al.
Tetrahedron, 1971 , vol. 27, p. 5683 - 5696
反应条件
1: sulfur; water; ammonium polysulfide / <185 2: sulfuric acid; aqueous sodium nitrite View Scheme
参考文献
Heilmann et al.
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1952 , vol. 235, p. 544
反应条件
1: diethyl ether 2: CuSO4-pumice stone / 200 °C / 200 Torr / Hydrieren des erhaltenen Olefingemisches an Nickel-Kieselgur bei 110-130grad und 84 at View Scheme
参考文献
Moersch; Whitmore
Journal of the American Chemical Society, 1949 , vol. 71, p. 820