α-D(+)-五乙酰葡萄糖合成路线 (共 168 条)
反应条件
montmorillonite K-10 6 h; Ambient temperature;
参考文献
Tetrahedron Letters, , vol. 39, # 15 p. 2215 - 2218
反应条件
T=20°C; pH=12; aq. phosphate buffer;
参考文献
Rapid Communications in Mass Spectrometry, , vol. 26, # 11 p. 1372 - 1376
反应条件
pyridine Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 112, # 9 p. 511 - 514
反应条件
pyridine; hydrogenchloride 1.) r.t., 48 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 112, # 9 p. 511 - 514
反应条件
sodium nitrite 1 h; Ambient temperature; Title compound not separated from byproducts;
参考文献
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, , vol. 37, # 1 p. 72 - 74
反应条件
in methanol; acetonitrile electrochemical synthesis: one compartment, three-electrode, air-tight cell, vitrous carbon anode and Pt catode, 0.2 M LiClO4 as supporting electrolyte, constant potential 1.34 V (vs standard calomel reference electrode); Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Carbohydrate Chemistry, , vol. 14, # 8 p. 1217 - 1236
反应条件
in methanol; acetonitrile electrochemical synthesis: one compartment, three-electrode, air-tight cell, vitrous carbon anode and Pt catode, 0.2 M LiClO4 as supporting electrolyte, constant potential 1.20 V (vs standard calomel reference electrode); Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Carbohydrate Chemistry, , vol. 14, # 8 p. 1217 - 1236
反应条件
sulfuric acid in acetic acid T=25°C; 24 h; var. reaction time; Rate constantProduct distributionMechanism;
参考文献
Carbohydrate Research, , vol. 279, p. 107 - 116
反应条件
trifluoroacetic acid 1) CH2Cl2, 18 deg C, 20 min, 2) pyridine, 24 h; Yield given. Multistep reaction;
参考文献
Chemische Berichte, , vol. 114, # 5 p. 1636 - 1648
反应条件
in acetonitrile electrochemical synthesis: one compartment, three-electrode, air-tight cell, vitrous carbon anode and Pt catode, 0.2 M LiClO4 as supporting electrolyte, constant potential 1.20 V (vs standard calomel reference electrode); Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Carbohydrate Chemistry, , vol. 14, # 8 p. 1217 - 1236