2,2-二乙氧基乙酸乙酯合成路线 (共 88 条)
参考文献
Horner et al.
Justus Liebigs Annalen der Chemie, 1953 , vol. 579, p. 212,220
反应条件
TiI4 in acetonitrile T=-78°C;
参考文献
Chemistry Letters, , # 9 p. 888 - 889
反应条件
lithium methanolate in methanol T=80°C; 10 h; Product distribution / selectivity;
参考文献
DSM FINE CHEMICALS AUSTRIA NFG GMBH and CO KG
Patent: WO2005/87711 A1, 2005 ;
Location in patent: Example 9 ;
参考文献
Horner et al.
Justus Liebigs Annalen der Chemie, 1953 , vol. 579, p. 212,220
参考文献
Merck and Co.
Patent: US2158098 , 1937 ;
参考文献
Merck and Co. Inc.
Patent: US2158098 , 1937 ;
反应条件
ammonia in ethanol 48 h; Ambient temperature;
参考文献
Inami; Shiba
Bulletin of the Chemical Society of Japan, 1985 , vol. 58, # 1 p. 352 - 360
参考文献
Scheibler; Schmidt
Chemische Berichte, 1933 , vol. 66, p. 504,505
反应条件
(i) NH3, (ii) POCl3, Py, (iii) H2S, NH3; Multistep reaction;
参考文献
Toogood, Peter L.; Hollenbeck, Jessica J.; Lam, Huong M.; Li, Li
Bioorganic and Medicinal Chemistry Letters, 1996 , vol. 6, # 13 p. 1543 - 1546
反应条件
(i) NH3, (ii) POCl3, Py; Multistep reaction;
参考文献
McElvain; Clarke
Journal of the American Chemical Society, 1947 , vol. 69, p. 2660