1,2,3,6,7,11B-六氢-4H-吡嗪并[2,1-Alpha]异喹啉-4-酮合成路线 （共 24 条）
反应条件
acetic acid in methanol T=0 - 60°C; 3 h; Inert atmosphere;
参考文献
Molecules, , vol. 18, # 8 p. 9163 - 9178
反应条件
1: 4-methyl-morpholine / dichloromethane / 4 h / 20 °C
2: phosphoric acid / water / 0.33 h / 150 °C / |Microwave irradiation
3: sodium carbonate / dichloromethane / 2 h / 0 - 20 °C
View Scheme
参考文献
Cedillo-Cruz, Alberto; Aguilar, Maria Isabel; Flores-Alamo, Marcos; Palomares-Alonso, Francisca; Jung-Cook, Helgi
Tetrahedron Asymmetry, 2014 , vol. 25, # 2 p. 133 - 140
反应条件
in dichloromethane
T=0 - 20°C; Inert atmosphere;
参考文献
Wang, Wen-Long; Song, Li-Jun; Chen, Xia; Yin, Xu-Ren; Fan, Wen-Hua; Wang, Gu-Ping; Yu, Chuan-Xin; Feng, Bainian
Molecules, 2013 , vol. 18, # 8 p. 9163 - 9178
反应条件
in chloroform
T=20°C; 8 h;
参考文献
Laurent, Sophie A.-L.; Boissier, Jerome; Cosledan, Frederic; Gornitzka, Heinz; Robert, Anne; Meunier, Bernard
European Journal of Organic Chemistry, 2008 , # 5 p. 895 - 913
