(E)-3-(2-呋喃)丙烯腈合成路线 (共 27 条)
参考文献
Ried; Reitz
Chemische Berichte, 1956 , vol. 89, p. 2570,2573
反应条件
1: aq. NaOH solution; hydroxylamine
2: water
View Scheme
参考文献
Ried; Reitz
Chemische Berichte, 1956 , vol. 89, p. 2570,2573
反应条件
sodium hydride
1.) DME, 15 deg C, 1 h, 2.) 60 deg C, 2 h; Multistep reaction. Title compound not separated from byproducts;
参考文献
Gregory, Barrie; Hinz, Werner; Jones, R. Alan; Arques, Jose Sepulveda
Journal of Chemical Research, Miniprint, 1984 , # 10 p. 2801 - 2821
反应条件
potassium hydroxide in water
T=60°C; var. of base, amount of H2O, rate of stirring, condition of KOH, solvent, without Me3SI; Product distributionMechanism;
参考文献
Bentley, T. William; Jones, Ray V. H.; Larder, Annette H.; Lock, Stephen J.
Journal of the Chemical Society, Chemical Communications, 1994 , # 19 p. 2309 - 2310
反应条件
potassium hydroxide
T=60°C; condensation of diaryl ketones with acetonitrile in the presence of KOH; temperature dependence; effect of water, phase transfer catalysts, cosolvent; kinetics and mechanism; Rate constantProduct distribution;
参考文献
Bentley, T. William; Jones, Ray V. H.; Larder, Annette H.; Lock, Stephen J.
Journal of the Chemical Society. Perkin Transactions 2, 1998 , # 1 p. 89 - 94
参考文献
Osipova, M. P.; Volkova, R. V.; Spiridonov, E. A.
J. Gen. Chem. USSR (Engl. Transl.), 1986 , vol. 56, # 2 p. 328 - 330,285 - 286
参考文献
Ried; Reitz
Chemische Berichte, 1956 , vol. 89, p. 2570,2573