sodium hydroxide; 5,11,17,23-tetramethoxy-25,26,27,28-tetrakis(trimethylammoniomethyl)calixlt;4gt;arene tetrachloride in water
T=20°C; Michael addition; 0.2 h;
piperidine in ethanol
Michael addition; 0.133333 h; microwave irradiation;
参考文献
Laskar, Dhrubojyoti D.; Prajapati, Dipak; Sandhu, Jagir S.
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2003 , vol. 42, # 1 p. 135 - 139
Connor; Andrews
Journal of the American Chemical Society, 1934 , vol. 56, p. 2713,2714
Full Text Show Details
Hauser; Abramovitch
Journal of the American Chemical Society, 1940 , vol. 62, p. 1763,1764
1: With 3-ethyl-5-(2-hydroxyethyl)-4-methyl-1,3-thiazolium bromide; 1,8-diazabicyclo[5.4.0]undec-7-ene; isopropyl alcohol in tetrahydrofuran
T=70°C;
2: With acetic acid in tetrahydrofuran
T=70°C;
参考文献
Mattson, Anita E.; Bharadwaj, Ashwin R.; Zuhl, Andrea M.; Scheidt, Karl A.
Journal of Organic Chemistry, 2006 , vol. 71, # 15 p. 5715 - 5724
