[Ru2(p-PriC6H4Me)2(μ-Cl)Cl]2; triethylamine; bis[2-(diphenylphosphino)phenyl] ether in toluene T=20°C; Inert atmosphereReflux;
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[(C5Me5)IrI2]2 in water T=115°C; 10 h; Inert atmosphere;
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Saidi, Ourida; Blacker, A. John; Farah, Mohamed M.; Marsden, Stephen P.; Williams, Jonathan M. J.
Chemical Communications, 2010 , vol. 46, # 9 p. 1541 - 1543
Walker, Daniel Patrick; Piotrowski, David W.; Jacobsen, Eric Jon; Acker, Brad A.; Myers, Jason K.; Groppi JR., Vincent E.
Patent: US2003/236279 A1, 2003 ;
Location in patent: Page 30 ;
[(C5Me5)IrI2]2 in water T=115°C; 10 h; Inert atmosphere;
参考文献
Saidi, Ourida; Blacker, A. John; Farah, Mohamed M.; Marsden, Stephen P.; Williams, Jonathan M. J.
Chemical Communications, 2010 , vol. 46, # 9 p. 1541 - 1543
1: 1-amino-1-phenylethane With cycloundeca[b]pyrimido[5,4-d]pyrrole12,14-dione derivative in acetonitrile 16 h; Irradiation; 2: (2,4-dinitro-phenyl)-hydrazine With hydrogenchloride
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[(C5Me5)IrI2]2 in water T=115°C; 10 h; Inert atmosphere;
参考文献
Saidi, Ourida; Blacker, A. John; Farah, Mohamed M.; Marsden, Stephen P.; Williams, Jonathan M. J.
Chemical Communications, 2010 , vol. 46, # 9 p. 1541 - 1543
1: 4 h / 160 °C 2: lithium aluminium tetrahydride / diethyl ether / 2 h / 50 °C / Heating / reflux View Scheme
参考文献
Walker, Daniel Patrick; Piotrowski, David W.; Jacobsen, Eric Jon; Acker, Brad A.; Myers, Jason K.; Groppi JR., Vincent E.
Patent: US2003/236279 A1, 2003 ;