1,2,3,4-四氢喹啉合成路线 (共 372 条)
反应条件
oxygen in para-xylene T=110°C; 3.5 h;
参考文献
Furukawa, Shinya; Suga, Akifusa; Komatsu, Takayuki
Chemical Communications, 2014 , vol. 50, # 25 p. 3277 - 3280
反应条件
rhenium sulfide in methanol; sodium hydroxide; chloroform; water; acetic acid
参考文献
EXXON RESEARCH AND ENGINEERING COMPANY
Patent: EP328319 A1, 1989 ;
反应条件
dihydrogen peroxide; copper dichloride in methanol 20 h; Ambient temperature; Yields of byproduct given;
参考文献
Murahashi, Shun-Ichi; Oda, Tetsuya; Sugahara, Toshiaki; Masui, Yoshiyuki
Journal of Organic Chemistry, 1990 , vol. 55, # 6 p. 1744 - 1749
反应条件
dihydrogen peroxide; sodium tungstate in methanol 24 h; Ambient temperature;
参考文献
Journal of Organic Chemistry, , vol. 55, # 6 p. 1744 - 1749
反应条件
4 A molecular sieve; 4-methylmorpholine N-oxide; tetrapropylammonium perruthennate in acetonitrile 6 h; Ambient temperature;
参考文献
Tetrahedron Letters, , vol. 35, # 35 p. 6567 - 6570
反应条件
[Ni(1,2-bis(di-isopropylphosphino)ethane)(μ-H)]2 in 1,4-dioxane T=180°C; 72 h; Inert atmosphere;
参考文献
Reyes-Sanchez, Adan; Canavera-Buelvas, Farrah; Barrios-Francisco, Rigoberto; Cifuentes-Vaca, Olga L.; Flores-Alamo, Marcos; Garcia, Juventino J.
Organometallics, 2011 , vol. 30, # 12 p. 3340 - 3345
反应条件
C18H32ClIrOP2S; sodium t-butanolate in para-xylene T=120°C; 12 h; Inert atmosphereSchlenk techniqueGloveboxSealed tube;
参考文献
Yao, Wubing; Zhang, Yuxuan; Jia, Xiangqing; Huang, Zheng
Angewandte Chemie - International Edition, 2014 , vol. 53, # 5 p. 1390 - 1394
Angew. Chem., 2014 , vol. 126, # 5 p. 1414 - 1418
反应条件
hydrogen; sulfided NiMo-Al2O3 in n-heptane T=349.9°C; P=52504.2 Torr; 2 h; effect of the partial pressure of title compound; reaction in the presence of 2,6-diethylaniline; Product distributionMechanism;
参考文献
Bulletin des Societes Chimiques Belges, , vol. 100, # 11 p. 801 - 806
反应条件
palladium 10 on activated carbon T=150°C; 24 h; Autoclave;
参考文献
Organic and Biomolecular Chemistry, , vol. 10, # 9 p. 1826 - 1833
反应条件
hydrogen; nickel T=210°C; P=7600 Torr; or 200 deg C, or Ru/C, 100 or 10 atm, 150 deg C, and competitive hydrogenation with 1,2,3,4-tetrahydroisoquinoline; Rate constant;
参考文献
Okazaki, Hiroshi; Onishi, Kiyotaka; Soeda, Mahito; Ikefuji, Yoshio; Tamura, Ryuji; Mochida, Isao
Bulletin of the Chemical Society of Japan, 1990 , vol. 63, # 11 p. 3167 - 3174