2,5-环己二烯-1,4-二酮单肟合成路线 （共 96 条）
反应条件
1: 87 percent / hydrogen chloride gas / 25 - 30 °C 2: 92 percent / 1.) conc. hydrochloric acid, sodium nitrite, 2.) phosphinous acid / dioxane; H2O / 20 h / 0 °C 3: 2.0 g / phosphoryl chloride / 0 deg C; room temperature, 0.5 h; 3 h View Scheme
参考文献
Sargent, Melvyn V.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 1095 - 1098
参考文献
van Erp
Recueil des Travaux Chimiques des Pays-Bas, 1911 , vol. 30, p. 302
反应条件
hydrogenchloride in diethyl ether T=-10 - 0°C; 1 h;
参考文献
Journal of Medicinal Chemistry, , vol. 47, # 11 p. 2816 - 2825
反应条件
hydrogenchloride T=25 - 30°C;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1095 - 1098
参考文献
Holliday and Co., Shaw
Patent: DE533129 , 1927 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 18, p. 558
反应条件
T=100 - 125°C; P=73550.8 - 110326 Torr; Hydrogenation;
参考文献
Cusmano
Atti della Accademia Nazionale dei Lincei, Classe di Scienze Fisiche, Matematiche e Naturali, Rendiconti, 1917 , vol. <5> 26 II, p. 89
反应条件
T=100 - 125°C; P=150 - 73550.8 Torr; Hydrogenation;
参考文献
Winans; Adkins
Journal of the American Chemical Society, 1933 , vol. 55, p. 2051,2056
反应条件
T=100 - 125°C; P=150 - 73550.8 Torr; Hydrogenation;
参考文献
Winans; Adkins
Journal of the American Chemical Society, 1933 , vol. 55, p. 2051,2056
参考文献
Matsumura; Sone
Journal of the American Chemical Society, 1931 , vol. 53, p. 1406
反应条件
T=500 - 540°C; bei der trocknen Destillation;
参考文献
Ray; Dutt
Journal of the Indian Chemical Society, 1928 , vol. 5, p. 106
Chem. Zentralbl., 1928 , vol. 99, # I p. 2370
