2,5-环己二烯-1,4-二酮单肟合成路线 （共 96 条）
反应条件
bei der Reduktion mit alkal. Mitteln;
参考文献
Vidal
Chemiker-Zeitung, Chemische Apparatur, 1905 , vol. 29, p. 487
Chem. Zentralbl., 1905 , vol. 76, # I p. 1316
参考文献
Plancher
Gazzetta Chimica Italiana, 1895 , vol. 25 II, p. 393
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Plancher
Gazzetta Chimica Italiana, vol. 25, p. II, 383
参考文献
Baeyer; Caro
Chemische Berichte, 1874 , vol. 7, p. 972
参考文献
Fischer; Wacker
Chemische Berichte, vol. 21, p. 2616
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Fischer,O.; Wacker
Chemische Berichte, 1888 , vol. 21, p. 2614
反应条件
1: 87 percent / hydrogen chloride gas / 25 - 30 °C 2: 92 percent / 1.) conc. hydrochloric acid, sodium nitrite, 2.) phosphinous acid / dioxane; H2O / 20 h / 0 °C View Scheme
参考文献
Sargent, Melvyn V.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 1095 - 1098
反应条件
hydrogenchloride in diethyl ether T=-10 - 0°C; 1 h;
参考文献
Kenny, Jane R.; Maggs, James L.; Meng, Xiaoli; Sinnott, Deborah; Clarke, Stephen E.; Park, B. Kevin; Stachulski, Andrew V.
Journal of Medicinal Chemistry, 2004 , vol. 47, # 11 p. 2816 - 2825
反应条件
hydrogenchloride; methanol T=0°C;
参考文献
Jaeger
Chemische Berichte, 1875 , vol. 8, p. 897
参考文献
Jaeger
Chemische Berichte, 1875 , vol. 8, p. 897
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Bargellini; Leone
Atti della Accademia Nazionale dei Lincei, Classe di Scienze Fisiche, Matematiche e Naturali, Rendiconti, 1928 , vol. <6>8, p. 399
Chem. Zentralbl., 1929 , vol. 100, # I p. 1441
反应条件
1: 45 percent / HCl (gas) / diethyl ether / 1 h / -10 - 0 °C 2: 82 percent / K2CO3; CuI; Cu / toluene / 48 h / Heating 3: 81 percent / BBr3 / CH2Cl2; 1,2-dichloro-ethane / 1 h / 20 °C 4: 70 percent / aq. NaOH / ethanol / 12 h / Heating View Scheme
参考文献
Kim, Sang-Hyun; Kwon, Jung-Hwan; Yoon, Sung-Hwa
Bulletin of the Korean Chemical Society, 2010 , vol. 31, # 10 p. 3007 - 3009
反应条件
in diethyl ether 0 deg C, 0.5 h then 20 deg C, 2 h;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 58, # 8 p. 1768 - 1778,1578 - 1586
