Ringold et al.
Journal of the American Chemical Society, 1959 , vol. 81, p. 3712,3715
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de Ruggieri et al.
Annali di Chimica (Rome, Italy), 1959 , vol. 49, p. 1371,1376
Bowlus; Nieuwland
Journal of the American Chemical Society, 1931 , vol. 53, p. 3836
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Meerwein; Pannwitz
Journal fuer Praktische Chemie (Leipzig), 1934 , vol. <2>141, p. 131,145
nitric acid in nitric acid; acetic acid boiling Pd-sponge in mixt. of glacial AcOH and concd. HNO3 (100:3 v/v), addn. of further Pd to end of evolution of N-oxides (if necessary); hot filtration, cooling (crystn.), washing (AcOH, water), drying in air;
参考文献
Beattie, James K.; MacLeman, Susan; Masters, Anthony F.
Inorganica Chimica Acta, 1999 , vol. 294, # 1 p. 99 - 102
in water; acetic acid Pd(II) nitrate dissolved in mixt. of acetic acid and H2O; mixt. stirred for 3 h at room temp.; filtered; washed (glacial acetic acid, ether); dried (vac. over alkali);mixt. extd. (benzene); filtered; filtrate evapd. to dryness at 40.degre e.C in vac.; elem. anal.;
参考文献
Stolyarov; Demina; Cherkashina
Russian Journal of Inorganic Chemistry, 2011 , vol. 56, # 10 p. 1532 - 1537