3,4,5-三甲氧基甲苯合成路线 （共 96 条）
反应条件
hydrogenchloride; hydrogen; palladium on activated charcoal T=20°C; P=760.051 Torr; 0.133333 h;
参考文献
Tetrahedron, , vol. 63, # 38 p. 9382 - 9386
反应条件
copper(l) chloride in methanol; N,N-dimethyl-formamide T=70 - 105°C; 7 h;
参考文献
Sankaranarayanan, Ananthakrishnan; Chandalia
Organic Process Research and Development, 2006 , vol. 10, # 3 p. 487 - 492
参考文献
Sumikin Chemical Co.
Patent: US5354899 A1, 1994 ;
反应条件
lithium aluminium tetrahydride; hydrogen; palladium on activated charcoal 1.) Et2O; 2.) ethanol, 1 atm; Multistep reaction;
参考文献
Magnetic Resonance in Chemistry, , vol. 25, p. 824 - 828
反应条件
1: diethyl ether 2: 1.) lithium aluminium hydride; 2.) H2 / 2.) 10percent Pd-C / 1.) Et2O; 2.) ethanol, 1 atm View Scheme
参考文献
Magnetic Resonance in Chemistry, , vol. 25, p. 824 - 828
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium carbonate in ethylene glycol dimethyl ether; water Suzuki-Miyaura Coupling; Inert atmosphereReflux;
参考文献
Wang, Xin; Fu, Jian-Min; Snieckus, Victor
Helvetica Chimica Acta, 2012 , vol. 95, # 12 p. 2680 - 2694
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium carbonate in ethylene glycol dimethyl ether; water Suzuki-Miyaura Coupling; Inert atmosphereReflux;
参考文献
Wang, Xin; Fu, Jian-Min; Snieckus, Victor
Helvetica Chimica Acta, 2012 , vol. 95, # 12 p. 2680 - 2694
反应条件
1: With naphthalene; lithium in tetrahydrofuran T=-50°C; 16 h; 2: With water in tetrahydrofuran T=20°C; Further stages.;
参考文献
Tetrahedron, , vol. 63, # 48 p. 11998 - 12006
反应条件
N,N,N',N'-tetramethyl-7,8-dihydro-6H-dipyrido[1,2-a;2',1'-c][1,4] diazepine-2,12-diamine in N,N-dimethyl-formamide 24 h; Inert atmosphereGloveboxUV-irradiation;
参考文献
Angewandte Chemie - International Edition, , vol. 52, # 8 p. 2239 - 2242
Angew. Chem., , vol. 125, # 8 p. 2295 - 2298,4
反应条件
1: With naphthalene; lithium in tetrahydrofuran T=-20°C; 5 h; 2: With water in tetrahydrofuran T=20°C; Further stages.;
参考文献
Tetrahedron, , vol. 63, # 48 p. 11998 - 12006
