氯化-1-乙基-3-甲基咪唑合成路线 （共 29 条）
反应条件
in neat (no solvent) (He); mixing iron compd. and imidazolium deriv. in molar ratio 1:1 at room temp., stirring at room temp. for 2 d; elem. anal.;
参考文献
Yoshida, Yukihiro; Otsuka, Akihiro; Saito, Gunzi; Natsume, Seiichi; Nishibori, Eiji; Takata, Masaki; Sakata, Makoto; Takahashi, Masahide; Yoko, Toshinobu
Bulletin of the Chemical Society of Japan, 2005 , vol. 78, # 11 p. 1921 - 1928
反应条件
in melt in acidic imidazolium/AlCl3 ionic melt at 25°C; not isolated, detd. by (51)V-NMR and IR spectroscopy;
参考文献
Bell; Castleman Jr.; Thorn
Inorganic Chemistry, 1999 , vol. 38, # 25 p. 5709 - 5715
反应条件
in water T=25°C; 3 h;
参考文献
Velazquez, Carlos A.; Lynn, Geoffrey M.; Kumar, Vineet; Keefer, Larry K.; Malhotra, Sanjay V.
Synthetic Communications, 2010 , vol. 40, # 9 p. 1322 - 1332
反应条件
T=110 - 115°C; P=750.075 - 1125.11 Torr; 72 h;
参考文献
Ignatyev, Nikolai (Mykola); Welz-Biermann, Urs; Kucheryna, Andriy; Willner, Helge
Patent: US2008/221334 A1, 2008 ;
Location in patent: Page/Page column 9 ;
参考文献
Green Chemistry, , vol. 14, # 10 p. 2738 - 2746,9
Green Chemistry, , vol. 14, # 10 p. 2738 - 2746
反应条件
1: potassium tert-butylate; 1-ethyl-3-methyl-1H-imidazolium chloride in butan-1-ol T=20°C; 3 h; 2: acetic acid in butan-1-ol Product distribution / selectivity;
参考文献
WO2005/70896 A1, ;
Page/Page column 20-21 ;
反应条件
1: sodium methylate; 1-ethyl-3-methyl-1H-imidazolium chloride in ethanol T=20°C; 0.5 h; 2: acetic acid in ethanol Product distribution / selectivity;
参考文献
WO2005/70896 A1, ;
Page/Page column 21 ;
反应条件
tetrafluoroboric acid in water T=20°C;
参考文献
WO2006/7912 A1, ;
Page/Page column 21-22 ;
参考文献
Green Chemistry, , vol. 12, # 10 p. 1711 - 1714
参考文献
Ignatyev, Nikolai (Mykola); Bissky, German; Willner, Helge
Patent: US2009/36628 A1, 2009 ;
Location in patent: Page/Page column 13 ;
