(S)-6,6'二溴-1,1'-联-2-萘酚合成路线 （共 10 条）
反应条件
bromine in dichloromethane T=-78°C; Inert atmosphere;
参考文献
Bunzen, Jens; Bruhn, Torsten; Bringmann, Gerhard; Luetzen, Arne
Journal of the American Chemical Society, 2009 , vol. 131, p. 3621 - 3630
反应条件
oxygen; C26H28N2O9V2 in tetrachloromethane T=0°C; 96 h; Product distribution / selectivity;
参考文献
Chengdu Institute of Organic Chemistry Chinese Academy of Sciences
Patent: US2005/256345 A1, 2005 ;
Location in patent: Page/Page column 2-3; 5 ;
反应条件
air; (NO+)Ru(II)-salen in toluene T=25°C; Arylation; 24 h; Irradiation; Product distribution; Further Variations:various amount of catalyst;
参考文献
Synlett, , # 10 p. 1433 - 1436
反应条件
cellulose tris(3,5-dichlorophenylcarbamate) enantioseparation of racemate;
参考文献
Chemistry Letters, , # 4 p. 352 - 353
反应条件
C136H102Fe2N4O6 in toluene T=60°C; 24 h; optical yield given as percent eeenantioselective reaction;
参考文献
Egami, Hiromichi; Matsumoto, Kenji; Oguma, Takuya; Kunisu, Takashi; Katsuki, Tsutomu
Journal of the American Chemical Society, 2010 , vol. 132, # 39 p. 13633 - 13635
反应条件
C136H102Fe2N4O6 in toluene T=60°C; 48 h; optical yield given as percent eeenantioselective reaction;
参考文献
Egami, Hiromichi; Matsumoto, Kenji; Oguma, Takuya; Kunisu, Takashi; Katsuki, Tsutomu
Journal of the American Chemical Society, 2010 , vol. 132, # 39 p. 13633 - 13635
参考文献
Bulletin of the Chemical Society of Japan, , vol. 66, # 7 p. 2002 - 2005
反应条件
Pseudomonas fluorescens lipoprotein lipase in isopropyl alcohol; acetone T=40°C; 126 h; Title compound not separated from byproducts;
参考文献
Tetrahedron Asymmetry, , vol. 14, # 3 p. 289 - 291
反应条件
C136H102Fe2N4O6 in toluene T=60°C; 48 h; optical yield given as percent eeenantioselective reaction;
参考文献
Egami, Hiromichi; Matsumoto, Kenji; Oguma, Takuya; Kunisu, Takashi; Katsuki, Tsutomu
Journal of the American Chemical Society, 2010 , vol. 132, # 39 p. 13633 - 13635
反应条件
1: (R)-6,6'-dibromo-BINOL With n-butyllithium in tetrahydrofuran; hexane T=-78 - -70°C; 5 h; Inert atmosphere; 2: carbonic acid dimethyl ester in tetrahydrofuran; hexane T=-78 - -40°C; 1.5 h; Inert atmosphere; 3: With hydrogenchloride in tetrahydrofuran; hexane; water T=20°C; pH=< 1; Cooling with ice;
参考文献
Verga, Daniela; Percivalle, Claudia; Doria, Filippo; Porta, Alessio; Freccero, Mauro
Journal of Organic Chemistry, 2011 , vol. 76, # 7 p. 2319 - 2323
