1-(三甲基硅氧烷)环己烯合成路线 (共 370 条)
反应条件
bis(acetylacetonate)nickel(II) in diethyl ether Heating;
参考文献
Hayashi, Tamio; Katsuro, Yoshio; Kumada, Makoto
Tetrahedron Letters, 1980 , vol. 21, p. 3915 - 3918
反应条件
bis(acetylacetonate)nickel(II) in diethyl ether 20 h; Ambient temperature;
参考文献
Hayashi, Tamio; Katsuro, Yoshio; Kumada, Makoto
Tetrahedron Letters, 1980 , vol. 21, p. 3915 - 3918
反应条件
fluorine in various solvent(s) T=-78°C; 3.5 h;
参考文献
Purrington, Suzane T.; Lazaridis, Nicholas V.; Bumgardner, Carl L.
Tetrahedron Letters, 1986 , vol. 27, # 24 p. 2715 - 2716
反应条件
BnNMe3(+)F(-) in tetrahydrofuran 16 h; Ambient temperature;
参考文献
Hirsch, Elisabeth; Huenig, Siegfried; Reissig, Hans-Ulrich
Chemische Berichte, 1982 , vol. 115, # 12 p. 3687 - 3696
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran 16 h; Ambient temperature;
参考文献
Hirsch, Elisabeth; Huenig, Siegfried; Reissig, Hans-Ulrich
Chemische Berichte, 1982 , vol. 115, # 12 p. 3687 - 3696
反应条件
T=375°C; other temperatures, ΔG(activ.), ΔH(excit.), ΔS(excit.), kinetic isotope effect; MechanismKineticsThermodynamic data;
参考文献
Schaffer, Frank; Beckhaus, Hans-Dieter; Rieger, Hans-Juergen; Ruechardt, Christoph
Chemische Berichte, 1994 , vol. 127, # 3 p. 557 - 564
反应条件
oxygen; silica gel; palladium in N,N-dimethyl acetamide T=67.9°C; 24 h; Yields of byproduct given;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , # 7 p. 1113 - 1119
反应条件
diallyl carbonate; palladium diacetate; 1,2-bis-(diphenylphosphino)ethane in acetonitrile 30 h; Heating;
参考文献
Tetrahedron Letters, , vol. 24, # 50 p. 5635 - 5638
反应条件
oxygen; silica gel; palladium in various solvent(s) T=59.9°C; 24 h;
参考文献
Journal of the Chemical Society - Series Chemical Communications, , # 22 p. 1697 - 1699
反应条件
in dichloromethane Irradiationother solvent, also in presence of Bu4NPF6; Quantum yieldProduct distributionMechanism;
参考文献
Journal of the Chemical Society. Perkin Transactions 2, , vol. 8, p. 1623 - 1632