1-(三甲基硅氧烷)环己烯合成路线 (共 370 条)
参考文献
Blaney; Grigg; Rankovic; Thoroughgood
Tetrahedron Letters, 2000 , vol. 41, # 34 p. 6639 - 6642
反应条件
bismuth(III) chloride; sodium iodide in dichloromethane 5 h; Ambient temperature; Yields of byproduct given;
参考文献
Peidro, Laurence; Le Roux, Christophe; Laporterie, Andre; Dubac, Jacques
Journal of Organometallic Chemistry, 1996 , vol. 521, # 1-2 p. 397 - 399
反应条件
tri-tert-butyl phosphine; tri-n-butyltin fluoride; tris(dibenzylideneacetone)dipalladium (0) in benzene 21 h; Heating;
参考文献
Iwama, Tetsuo; Rawal, Viresh H.
Organic Letters, 2006 , vol. 8, # 25 p. 5725 - 5728
反应条件
tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; tri-n-butyltin fluoride in benzene 24 h; Inert atmosphereReflux;
参考文献
Cheon, Cheol Hong; Imahori, Tatsushi; Yamamoto, Hisashi
Chemical Communications, 2010 , vol. 46, # 37 p. 6980 - 6982
反应条件
samarium (III) iodide in tetrahydrofuran T=80°C; 4 h;
参考文献
Bao, Weiliang; Zhang, Yongmin; Ying, Taokai
Synthetic Communications, 1996 , vol. 26, # 3 p. 503 - 507
反应条件
antimony trichloride in dichloromethane T=0°C; 1 h;
参考文献
Journal of Organic Chemistry, , vol. 47, # 26 p. 5099 - 5102
反应条件
bismuth(III) chloride; sodium iodide in diethyl ether; dichloromethane 1 h; Ambient temperatureother acid chlorides, other trimethylsilyl enol ethers, other reagents: ZnCl2, SbCl3, SbCl5, SnCl4, sodium iodide absence, zinc iodide presence, other reaction time; MechanismProduct distribution;
参考文献
Journal of Organic Chemistry, , vol. 61, # 11 p. 3885 - 3887
反应条件
DTPP-F6 Yield given. Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 45, # 25 p. 5052 - 5057
反应条件
in nitromethane T=-35°C; 1 h;
参考文献
Journal of Organic Chemistry, , vol. 46, # 19 p. 3771 - 3773
反应条件
1: With dimethylsulfide borane complex in tetrahydrofuran T=20°C; 4 h; 2: With benzene-1,2-diol; triethylamine in tetrahydrofuran T=20°C; 2.5 h; 3: With oxygen in tetrahydrofuran T=20°C; 12 h;
参考文献
Cadot, Christine; Dalko, Peter I.; Cossy, Janine
Tetrahedron Letters, 2001 , vol. 42, # 9 p. 1661 - 1663