2,2'-二甲氧基苯偶酰合成路线 (共 24 条)
反应条件
in tetrahydrofuran
T=-55°C; 16 h;
参考文献
Sibi, Mukund P.; Marvin, Mali; Sharma, Rajiv
Journal of Organic Chemistry, 1995 , vol. 60, # 16 p. 5016 - 5023
反应条件
water in acetonitrile
electrolysis at constant current 0.4 A in presence of Et4NOTs; in absence of H2O - 55percent;
参考文献
Okimoto, Mitsuhiro; Itoh, Toshiaki; Chiba, Toshiro
Journal of Organic Chemistry, 1996 , vol. 61, # 14 p. 4835 - 4837
反应条件
in tetrahydrofuran
T=-60°C; 8 h;
参考文献
Sibi; Sharma; Paulson
Tetrahedron Letters, 1992 , vol. 33, # 15 p. 1941 - 1944
反应条件
hydrogen bromide in dimethyl sulfoxide
参考文献
You, Lei; Cho, Eun Jeong; Leavitt, John; Ma, Li-Chung; Montelione, Gaetano T.; Anslyn, Eric V.; Krug, Robert M.; Ellington, Andrew; Robertus, Jon D.
Bioorganic and Medicinal Chemistry Letters, 2011 , vol. 21, # 10 p. 3007 - 3011
参考文献
Ranade, A. C.; Mali, R. S.; Kurnawal, V. M.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 6 p. 514 - 517
参考文献
Schoenberg; Kraemer
Chemische Berichte, 1922 , vol. 55, p. 1189
参考文献
Wittig; Gauss
Chemische Berichte, 1947 , vol. 80, p. 363,373
反应条件
TiI4 in acetonitrile
T=0 - 20°C; Reduction; 5.3 h;
参考文献
Hayakawa; Sahara; Shimizu
Tetrahedron Letters, 2000 , vol. 41, # 41 p. 7939 - 7942
反应条件
aluminium trichloride; nitrobenzene
T=55°C;
参考文献
Gee; Harley-Mason
Journal of the Chemical Society, 1947 , p. 251
反应条件
ammonium acetate in acetic acid
2 h; Heating;
参考文献
Liu, Yan; Sandoval, Christian A.; Yamaguchi, Yoshiki; Zhang, Xue; Wang, Zheng; Kato, Koichi; Ding, Kuiling
Journal of the American Chemical Society, 2006 , vol. 128, # 44 p. 14212 - 14213