2-羟基-5-甲氧基苯甲醛合成路线 （共 150 条）
反应条件
1: potassium persulfate; NaOH-solution; alkali / 30 - 35 °C / und Erhitzen des Reaktionsprodukts mit konz.Salzsaeure auf 70grad 2: aqueous NaOH-solution View Scheme
参考文献
Journal of the Chemical Society, , p. 2340
参考文献
Journal of the Chemical Society, , p. 2340
反应条件
(i) SOCl2, Py, PE, (ii) H2, quinoline, sulfur, Pd-BaSO4, xylene; Multistep reaction;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 40, p. 1428 - 1432
反应条件
in ein zuvor auf 165grad erhitztes Gemisch von Glycerin und Borsaeure bei 150grad und Behandeln des Reaktionsgemisches mit wss.H2SO4 bei 115grad;
参考文献
Iowa State College Journal of Science, , vol. 22, p. 91,108
参考文献
Chemische Berichte, , vol. 14, p. 1986
反应条件
1: potassium carbonate / N,N-dimethyl-formamide / 1.5 h / 140 °C / Molecular sieve 2: lithium aluminium tetrahydride / N,N-dimethyl-formamide; tetrahydrofuran / 0.17 h / 0 °C 3: phosphorus tribromide / N,N-dimethyl-formamide / 1 h / 0 °C View Scheme
参考文献
Korea Institute of Science and Technology; HANMI HOLDINGS CO., LTD
Patent: US2011/124888 A1, 2011 ;
反应条件
potassium carbonate in N,N-dimethyl-formamide T=140°C; 1.5 h; RefluxMolecular sieve;
参考文献
Korea Institute of Science and Technology; HANMI HOLDINGS CO., LTD
Patent: US2011/124888 A1, 2011 ;
Location in patent: Page/Page column 6 ;
反应条件
potassium carbonate in N,N-dimethyl-formamide T=90°C; 48 h;
参考文献
BIOLIPOX AB
Patent: WO2008/110793 A1, 2008 ;
Location in patent: Page/Page column 110 ;
反应条件
potassium carbonate in butanone 4 h; Heating;
参考文献
Friedman; Toyne; Goodby; Hird
Journal of Materials Chemistry, 2001 , vol. 11, # 11 p. 2759 - 2772
反应条件
bromine; sodium acetate in acetic acid T=20°C; 1 h;
参考文献
Evano, Gwilherm; Schaus, Jennifer V.; Panek, James S.
Organic Letters, 2004 , vol. 6, # 4 p. 525 - 528
