in ethanol; dichloromethane
under N2 to Mo(HB(Me2pyz)3)(NO)Br2 dissolved in dichloromethane added methylamine (33percent soln. in ethanol) and stirred at room temp. for 30 min; volume solvent reduced, Et2O added, (NH3Me)Br filtered off, volume filtrate reduced in vacuo; elem. anal.;
参考文献
Drane, A. Stephen; McCleverty, Jon A.
Polyhedron, 1983 , vol. 2, p. 53 - 58