反应条件
1: 1.) BH3*DMS, 2.) aq. 30percent H2O2, NaOH / 1.) THF, a) RT, 3 h, b) reflux, 1.5 h, 2.) THF, EtOH, RT, 2 h 2: 75 percent / pyridinium chlorochromate / CH2Cl2 / 5 h / Ambient temperature View Scheme
参考文献
Upadhya; Sudalai
Tetrahedron Asymmetry, 1997 , vol. 8, # 21 p. 3685 - 3689