2,3,5-三甲基苯酚合成路线 （共 124 条）
反应条件
1: H2SO4 2: 51 percent / ClSO3H / CH2Cl2 View Scheme
参考文献
Carpino, Louis A.; Shroff, Hitesh; Triolo, Salvatore A.; Mansour, El-Sayed M. E.; Wenschuh, Holger; Albericio, Fernando
Tetrahedron Letters, 1993 , vol. 34, # 49 p. 7829 - 7832
参考文献
Kolbezen et al.
Journal of Agricultural and Food Chemistry, 1954 , vol. 2, p. 864,865, 866
反应条件
sodium hydride in dimethyl sulfoxide 10 h; Ambient temperature;
参考文献
Fujino, Masahiko; Wakimasu, Mitsuhiro; Kitada, Chieko
Chemical & Pharmaceutical Bulletin, 1981 , vol. 29, # 10 p. 2825 - 2831
反应条件
potassium hydroxide 0.5 h; Heating;
参考文献
Bestmann; Ermann
1984 , vol. 1984, # 10 p. 1740 - 1745
反应条件
peracetic acid T=50°C; 0.25 h; Product distributionKineticsThermodynamic data;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 22, # 11 p. 2071 - 2078
Zhurnal Organicheskoi Khimii, , vol. 22, # 11 p. 2306 - 2315
反应条件
sulfuric acid T=50°C; 0.5 h; effect of catalysts; MechanismThermodynamic data;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 57, # 4 p. 923 - 930,819 - 826
反应条件
triethylamine in benzene T=5°C; 4 h;
参考文献
Nidiry, Eugene Sebastian J.; Roy, N. K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1988 , vol. 27, # 1-12 p. 1024 - 1028
反应条件
1: 1) NaOEt / 1) 5 min, 2a) 100 deg C, 5 h, 2b) 150 deg C, 12 h 2: 64 percent / PPA / 2.5 h / Heating 3: 81 percent / 4percent ethanolic KOH View Scheme
参考文献
Tripathi, Ravish C.; Tandon, V. K.; Khanna, J. M.; Saxena, Anil K.; Anand, Nitya
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1989 , vol. 28, # 1-11 p. 37 - 41
反应条件
1: 72 percent / base
2: 95 percent / SnCl4
3: 100 percent
4: 83 percent
5: 99 percent / LiAlH4
6: 20 percent / MnO2
View Scheme
参考文献
Makin, S. M.; Mikerin, I. E.; Dobretsova, E. K.; Shavrygina, O. A.
Russian Journal of Organic Chemistry, 1993 , vol. 29, # 4 p. 572 - 575
Zhurnal Organicheskoi Khimii, 1993 , vol. 29, # 4 p. 682 - 686
反应条件
1: benzene
2: aqueous hydrochloric acid; amalgamated zinc
View Scheme
参考文献
Smith; Holmes
Journal of the American Chemical Society, 1951 , vol. 73, p. 4294,4297
