[(3-丁烯-1-基氧基)甲基]苯合成路线 （共 32 条）
反应条件
ZnCl2*Et2O in dichloromethane
T=-78°C; 0.166667 h;
参考文献
Yamamoto, Yoshinori; Onuki, Setsuko; Yumoto, Masatoshi; Asao, Naoki
Heterocycles, 1998 , vol. 47, # 2 p. 765 - 780
反应条件
NaH in hexane; N,N-dimethyl-formamide
参考文献
Merck and Co., Inc.
Patent: US5120729 A1, 1992 ;
反应条件
in tetrahydrofuran
T=0°C; Grignard reaction; 0.5 h; Inert atmosphere;
参考文献
Taber, Douglass F.; Paquette, Craig M.; Reddy, P. Ganapati
Tetrahedron Letters, 2009 , vol. 50, # 21 p. 2462 - 2463
反应条件
trimethylsilyl iodide in acetonitrile
2.5 h; Ambient temperature;
参考文献
Sakurai, Hideki; Sakata, Yasuyuki; Hosomi, Akira
Chemistry Letters, 1983 , p. 409 - 412
反应条件
tetra-(n-butyl)ammonium iodide
参考文献
Ochiai, Masahito; Ito, Takao; Takahashi, Hideo; Nakanishi, Akinobu; Toyonari, Mika; Sueda, Takuya; Goto, Satoru; Shiro, Motoo
Journal of the American Chemical Society, 1996 , vol. 118, # 33 p. 7716 - 7730
反应条件
hydrogen in 1,4-dioxane; methanol
T=20°C; 24 h; chemoselective reaction;
参考文献
Sajiki, Hironao; Mori, Shigeki; Ohkubo, Tomoyuki; Ikawa, Takashi; Kume, Akira; Maegawa, Tomohiro; Monguchi, Yasunari
Chemistry - A European Journal, 2008 , vol. 14, # 17 p. 5109 - 5111
反应条件
sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate
参考文献
Nelson, Todd D.; Rosen, Jonathan D.; Smitrovich, Jacqueline H.; Payack, Joseph; Craig, Bridgette; Matty, Louis; Huffman, Mark A.; McNamara, James
Organic Letters, 2005 , vol. 7, # 1 p. 55 - 58
反应条件
1: titanium(IV) isopropylate With n-butyllithium in tetrahydrofuran
T=0°C; 0.0833333 h; Inert atmosphere;
2: ((but-3-en-1-yloxy)methyl)benzene in tetrahydrofuran
T=20°C; 0.5 h; Inert atmosphere;
3: carbon dioxide in tetrahydrofuran
T=0°C; 0.333333 h; Inert atmosphere;
参考文献
Rassadin, Valentin A.; Six, Yvan
Tetrahedron, 2014 , vol. 70, # 4 p. 787 - 794
反应条件
1: ((but-3-en-1-yloxy)methyl)benzene With titanium(IV) isopropylate; n-butyllithium in diethyl ether
T=0°C; 0.166667 h; Inert atmosphere;
2: carbon dioxide in diethyl ether
T=0°C; 0.333333 h; Inert atmosphere;
参考文献
Rassadin, Valentin A.; Six, Yvan
Tetrahedron, 2014 , vol. 70, # 4 p. 787 - 794
反应条件
1: phosphorous oxychloride; zinc-copper / diethyl ether / Heating
2: zinc; acetic acid / Heating
View Scheme
参考文献
Kabalka, George W.; Yao, Min-Liang; Navarane, Abhijit
Tetrahedron Letters, 2005 , vol. 46, # 29 p. 4915 - 4917
