in xylene at reflux 140-106°C for 165 h, then distilling butanol-borane azeotrop;
参考文献
Gmelin Handbook: B: B-Verb.1, 3.5.4.4, page 260 - 263
Full Text Show Details
U.S. Borax & Chemical Corp.
Patent: US3159590 , 1964 ;
C.A., 1965 , vol. 62, p. 11932
in xylene at reflux 140-106°C for 27 h, then distilling butanol-borane azeotrop;
参考文献
Gmelin Handbook: B: B-Verb.1, 3.5.4.4, page 260 - 263
Full Text Show Details
U.S. Borax & Chemical Corp.
Patent: US3159590 , 1964 ;
C.A., 1965 , vol. 62, p. 11932
in benzene to benzene soln. of nitrone of salicylaldehyde added (C6H4O2)BOC4H9 (molar ratio 1:1), refluxed for 30 min; concd. in vac., added petroleum ether, ppt. washed with ether, dried, elem. anal.;
参考文献
Kliegel, Wolfgang; Nanninga, Dierk
Journal of Organometallic Chemistry, 1983 , vol. 243, # 4 p. 373 - 386
