反应条件
in further solvent(s)
N2-atmosphere, 25percentstoich. excess of tetrafluorophthalonitrile, refluxing in 1-chloronaphtalene (24 h); cooling to room temp., filtration, addn. of petroleum ether, cooling in ice bath (pptn.), filtration, recrystn. (H2SO4);
参考文献
Balkus, Kenneth J.; Gabrielov, Alexei G.; Bell, Stephen L.; Bedioui, Fethi; Roue, Lionel; Devynck, Jacques
Inorganic Chemistry, 1994 , vol. 33, p. 67 - 72