2-叔丁基-1,3-二异丙基异脲合成路线 （共 19 条）
反应条件
in tetrahydrofuran T=55 - 60°C; 20.5 h;
参考文献
Tanaka, Ken-Ichi; Sawanishi, Hiroyuki
Tetrahedron Asymmetry, 1998 , vol. 9, # 1 p. 71 - 77
反应条件
Curtius rearrangement;
参考文献
Hodgson, David M.; Thompson, Alison J.; Wadman, Sjoerd
Tetrahedron Letters, 1998 , vol. 39, # 20 p. 3357 - 3358
反应条件
in dichloromethane 8 h; Heating;
参考文献
Matsuura, Fumiyoshi; Hamada, Yasumasa; Shioiri, Takayuki
Tetrahedron, 1993 , vol. 49, # 36 p. 8211 - 8222
反应条件
4 A molecular sieve; tin(IV) chloride in toluene
3 h; Heating; Yield given;
参考文献
Hodgson, David M.; Thompson, Alison J.; Wadman, Sjoerd
Tetrahedron Letters, 1998 , vol. 39, # 20 p. 3357 - 3358
反应条件
in dichloromethane; tert-butyl alcohol
T=20°C; 16 h;
参考文献
Maruoka, Hiroshi; Muto, Tsuyoshi; Tanaka, Taisaku; Imajo, Seiichi; Tomimori, Yoshiaki; Fukuda, Yoshiaki; Nakatsuka, Takashi
Bioorganic and Medicinal Chemistry Letters, 2007 , vol. 17, # 12 p. 3435 - 3439
反应条件
in dichloromethane; tert-butyl alcohol
T=20°C; 2 h;
参考文献
Sasaki, Shingo; Suzuki, Hiroto; Ouchi, Hitoshi; Asakawa, Tomohiro; Inai, Makoto; Sakai, Ryuichi; Shimamoto, Keiko; Hamashima, Yoshitaka; Kan, Toshiyuki
Organic Letters, 2014 , vol. 16, # 2 p. 564 - 567
反应条件
in acetonitrile
T=120°C; 0.0333333 h; Microwave irradiation;
参考文献
Chighine, Alessandra; Crosignani, Stefano; Arnal, Marie-Claire; Bradley, Mark; Linclau, Bruno
Journal of Organic Chemistry, 2009 , vol. 74, # 13 p. 4753 - 4762
反应条件
in 1,4-dioxane
T=20°C; 0.333333 h;
参考文献
Yu, Yanfei; Li, Zhengning; Jiang, Lan
Phosphorus, Sulfur and Silicon and the Related Elements, 2012 , vol. 187, # 5 p. 632 - 640
反应条件
4-(N,N-dimethlyamino)pyridine in tetrahydrofuran; hydrogenchloride; dichloromethane; water
参考文献
Gilead Sciences, Inc.
Patent: US2011/135599 A1, 2011 ;
US 20110135599 A1
