1-氯-2-亚甲基环己烷合成路线 （共 26 条）
反应条件
1: 8.6 g / Na2CO3, PAA / CH2Cl2 / 24 h / 20 °C
2: HCl / diethyl ether / 2 h / 13 °C
3: POCl3, pyridine
View Scheme
参考文献
Vereshchagin, A. N.; Kovylyaeva, G. I.; Bakaleinik, G. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1988 , vol. 37, # 1 p. 91 - 95
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1988 , # 1 p. 101 - 105
反应条件
1: LiAlH4 / diethyl ether
2: POCl3, pyridine
View Scheme
参考文献
Vereshchagin, A. N.; Kovylyaeva, G. I.; Bakaleinik, G. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1988 , vol. 37, # 1 p. 91 - 95
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1988 , # 1 p. 101 - 105
反应条件
chlorine bleach; water
T=0 - 8°C; 2 h; Further byproducts given. Yields of byproduct given;
参考文献
Vereshchagin, A. N.; Kovylyaeva, G. I.; Bakaleinik, G. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1988 , vol. 37, # 1 p. 91 - 95
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1988 , # 1 p. 101 - 105
反应条件
1: ethanol
2: aqueous KOH-solution
3: sulfuric acid
4: sodium; ethanol
5: PCl5 / 100 °C
View Scheme
参考文献
Mousseron; Jullien; Winternitz
Bulletin de la Societe Chimique de France, 1948 , p. 878,885
反应条件
1: aqueous KOH-solution
2: sulfuric acid
3: sodium; ethanol
4: PCl5 / 100 °C
View Scheme
参考文献
Mousseron; Jullien; Winternitz
Bulletin de la Societe Chimique de France, 1948 , p. 878,885
反应条件
1: sulfuric acid
2: sodium; ethanol
3: PCl5 / 100 °C
View Scheme
参考文献
Mousseron; Jullien; Winternitz
Bulletin de la Societe Chimique de France, 1948 , p. 878,885
反应条件
pyridine; trichlorophosphate
Title compound not separated from byproducts;
参考文献
Vereshchagin, A. N.; Kovylyaeva, G. I.; Bakaleinik, G. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1988 , vol. 37, # 1 p. 91 - 95
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1988 , # 1 p. 101 - 105
参考文献
Arnold; Lee
Journal of the American Chemical Society, 1953 , vol. 75, p. 5396,5399
参考文献
Mousseron; Jullien; Winternitz
Bulletin de la Societe Chimique de France, 1948 , p. 878,885
Show Details
Mousseron; Winternitz; Jullien
Bulletin de la Societe Chimique de France, 1947 , p. 80
参考文献
Mousseron; Jullien; Winternitz
Bulletin de la Societe Chimique de France, 1948 , p. 878,885
