(E)-2-丁烯基乙酸酯合成路线 (共 41 条)
反应条件
2,6-di-tert-butyl-4-methyl-phenol; ethane-1,2-disulfonic acid in water
T=60°C; 18 h; Product distribution / selectivity;
参考文献
BP CHEMICALS LIMITED
Patent: WO2003/82796 A1, 2003 ;
Location in patent: Page/Page column 13-22 ;
反应条件
4-(N,N-dimethlyamino)pyridine; triethylamine in dichloromethane
T=20°C; Inert atmosphere;
参考文献
Dubovyk, Igor; Watson, Iain D. G.; Yudin, Andrei K.
Journal of Organic Chemistry, 2013 , vol. 78, # 4 p. 1559 - 1575
反应条件
copper dichloride in benzene
T=70°C; 233 h; further reagents, solvents, reaction time; Product distribution;
参考文献
Beckwith,A.J.; Zavitsas,A.A.
Journal of the American Chemical Society, 1986 , vol. 108, p. 8230
反应条件
copper diacetate in benzene
T=70°C; 120 h; further reagents, solvents, reaction time; Product distribution;
参考文献
Beckwith,A.J.; Zavitsas,A.A.
Journal of the American Chemical Society, 1986 , vol. 108, p. 8230
反应条件
copper diacetate in benzene
T=70°C; 120 h; further reagents, solvents, reaction time; Product distribution;
参考文献
Beckwith,A.J.; Zavitsas,A.A.
Journal of the American Chemical Society, 1986 , vol. 108, p. 8230
反应条件
sodium nitrite
Deamination; ring cleavage; 1 h;
参考文献
Wiberg, Kenneth B.; Oesterle, Carmen G.
Journal of Organic Chemistry, 1999 , vol. 64, # 21 p. 7756 - 7762
参考文献
Kurth, Mark J.; Yu, Chan-Mo
Tetrahedron Letters, 1984 , vol. 25, # 44 p. 5003 - 5006
反应条件
tetrabutyl-ammonium chloride; potassium carbonate; palladium dichloride in N,N-dimethyl acetamide
T=100°C; 20 h;
参考文献
Liu, Yan; Yao, Bo; Deng, Chen-Liang; Tang, Ri-Yuan; Zhang, Xing-Guo; Li, Jin-Heng
Organic Letters, 2011 , vol. 13, # 5 p. 1126 - 1129
反应条件
trifluoroacetic acid; cobalt(II) dibromide; zinc in acetonitrile
T=20°C; 24 h;
参考文献
Gomes, Paulo; Gosmini, Corinne; Perichon, Jacques
Synthesis, 2003 , # 12 p. 1909 - 1915
反应条件
manganese; trifluoroacetic acid; zinc dibromide; FeBr2(bpy) in N,N-dimethyl-formamide
T=80°C; 5 h;
参考文献
Durandetti, Muriel; Gosmini, Corinne; Perichon, Jacques
Tetrahedron, 2007 , vol. 63, # 5 p. 1146 - 1153