5-乙酰基-2,2-二甲基-1,3-二恶烷-4,6-二酮合成路线 （共 28 条）
反应条件
1: 2,2-Dimethyl-[1,3]dioxane-4,6-dione With pyridine in dichloromethane 0.25 h; 2: acetyl chloride in dichloromethane T=0 - 20°C; 7 h;
参考文献
More; Mahulikar
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2006 , vol. 45, # 3 p. 823 - 825
反应条件
pyridine; 1,1'-carbonyldiimidazole 1.) CH2Cl2, RT, 6 h, 2.) CH2Cl2, RT, 48 h; Multistep reaction;
参考文献
Bioorganic and Medicinal Chemistry, , vol. 5, # 4 p. 749 - 764
反应条件
0.0666667 h; microwave irradiation;
参考文献
More; Mahulikar
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2006 , vol. 45, # 3 p. 823 - 825
反应条件
0.0833333 h; microwave irradiation;
参考文献
More; Mahulikar
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2006 , vol. 45, # 3 p. 823 - 825
反应条件
1: 5-acetyl-2,2-dimethyl-[1,3]dioxane-4,6-dione With alcohol Microwave irradiation; 2: urea 0.05 h; Microwave irradiation;
参考文献
More; Mahulikar
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2011 , vol. 50, # 5 p. 745 - 747
反应条件
aluminum isopropoxide T=160°C; Carroll Reaction; 6 h;
参考文献
COYOTE PHARMACEUTICALS, INC.; SERIZAWA, Hiroaki; ARGADE, Ankush B.; DATWANI, Akash; SPENCER, Natalie; PAN, Yonghua; ERMINI, Florian
Patent: WO2013/130654 A1, 2013 ;
Location in patent: Paragraph 0282; 0283 ;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 20, # 12 p. 3664 - 3668
反应条件
0.0666667 h; microwave irradiation;
参考文献
More; Mahulikar
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2006 , vol. 45, # 3 p. 823 - 825
反应条件
in benzene 0.5 h; Heating;
参考文献
Morita, Yasuo; Kaneko, Masakazu; Matsuzawa, Sumiko; Yamamoto, Yutaka
Journal of Heterocyclic Chemistry, 1997 , vol. 34, # 2 p. 515 - 519
反应条件
1: 5-acetyl-2,2-dimethyl-[1,3]dioxane-4,6-dione With alcohol Microwave irradiation; 2: thiourea 0.05 h; Microwave irradiation;
参考文献
More; Mahulikar
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2011 , vol. 50, # 5 p. 745 - 747
