1-甲氧基-4-苯基乙炔苯合成路线 （共 169 条）
反应条件
hydrogenchloride; zinc(II) chloride in dichloromethane 1 h; Ambient temperature;
参考文献
Chemische Berichte, , vol. 116, # 2 p. 777 - 797
反应条件
tetrabutyl-ammonium chloride; sodium acetate; palladium diacetate in N,N-dimethyl-formamide T=100°C; 24 h; Yield given. Yields of byproduct given;
参考文献
Larock, R. C.; Doty, M. J.; Cacchi, S.
Journal of Organic Chemistry, 1993 , vol. 58, # 17 p. 4579 - 4583
反应条件
hydroxytriphenylsilane; hexacarbonyl molybdenum in octane 0.166667 h; Irradiation;
参考文献
Finke, Aaron D.; Moore, Jeffrey S.
Chemical Communications, 2010 , vol. 46, # 42 p. 7939 - 7941
反应条件
N-iodo-succinimide; trimethylsilylazide in 1,2-dichloro-ethane; acetonitrile T=20 - 70°C; 3 h;
参考文献
Organic Letters, , vol. 15, # 11 p. 2571 - 2573
反应条件
C32H28BrFeIN3Pd; potassium acetate; silver(l) oxide in 1,2-dichloro-ethane
T=80°C; 24 h;
参考文献
Li, Hong-Mei; Xu, Chen; Duan, Lu-Meng; Lou, Xin-Hua; Wang, Zhi-Qiang; Li, Zhen; Fan, Yao-Ting
Transition Metal Chemistry, 2013 , vol. 38, # 3 p. 313 - 318
反应条件
copper(l) iodide; potassium carbonate; triphenylphosphine in water
T=100°C; 24 h; Inert atmosphere;
参考文献
Li, Tingyi; Sun, Peng; Yang, Hailong; Zhu, Yan; Yan, Hong; Lu, Linhua; Mao, Jincheng
Tetrahedron, 2012 , vol. 68, # 32 p. 6413 - 6419
反应条件
tetra-n-butylammonium acetate; [1-cyclohexyl-3-(di-pyridin-2-yl-methyl)-urea][PdCl2] in 1-methyl-pyrrolidin-2-one
T=110°C; 0.25 h;
参考文献
Gil-Molto, Juan; Najera, Carmen
Advanced Synthesis and Catalysis, 2006 , vol. 348, # 14 p. 1874 - 1882
反应条件
copper(l) iodide; 8-hydroxy-quinoline; sodium salt of phosphorous acid in ethanol
T=80°C; Suzuki coupling; 24 h;
参考文献
Wang, Shihua; Wang, Min; Wang, Lei; Wang, Bo; Li, Pinhua; Yang, Jin
Tetrahedron, 2011 , vol. 67, # 26 p. 4800 - 4806
反应条件
copper(l) iodide; 1,2-bis(diphenylphosphino)-1'-(diisopropylphosphino)-3',4-di-tert-butyl ferrocene; potassium carbonate; bis(η3-allyl-μ-chloropalladium(II)) in N,N-dimethyl-formamide
T=130°C; Sonogashira cross-coupling; 20 h;
参考文献
Hierso, Jean-Cyrille; Fihri, Aziz; Amardeil, Regine; Meunier, Philippe; Doucet, Henri; Santelli, Maurice
Tetrahedron, 2005 , vol. 61, # 41 p. 9759 - 9766
反应条件
potassium acetate; palladium diacetate; silver(l) oxide in dichloromethane
T=20°C; 12 h; Molecular sieve;
参考文献
Feng, Chao; Loh, Teck-Peng
Chemical Communications, 2010 , vol. 46, # 26 p. 4779 - 4781
