in diethylene glycol dimethyl ether
byproducts: H2; further intermediate: KSiH3; under N2, dispersion of potassium reacts with SiH4 at 100°C, concd. in vacuo at 30°C, C4F9SO3SiH3 added at -60°C, stored at this temp. for 10 min, warmed to 40°C; volatiles removed over 3 h in vacuo, SiH4 removed; GC;
in diethylene glycol dimethyl ether
byproducts: H2; further intermediate: KSiH3; under N2, dispersion of potassium reacts with SiH4 at 100°C, soln. of PhSO3H added dropwise at -40°C; volatiles removed at room temp. in vacuo, SiH4 removed; GC;
Cueilleron, J.
Bulletin de la Societe Chimique de France, 1945 , vol. 12, # 5 p. 88 - 89
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Gmelin Handbook: Ni: MVol.AI, 10.1, page 603 - 609
