in neat (no solvent, solid phase) elements and small quantity of SbI3 sealed in Ta container, heated in evacuated mullite tube (1300 ° C, 2 wks), vac. not adequate to maintain compositional integrity;
参考文献
Garcia, Eduardo; Corbett, John D.
Inorganic Chemistry, 1988 , vol. 27, p. 2353 - 2359
in neat (no solvent, solid phase) stoich. mixt. in evacuated and sealed silica tube heated up to 850°C, kept at this temp. for 120 h; cooled to 400°C at 5 K/h, quenched;
参考文献
Wiley, John B.; Poeppelmeier, Kenneth R.
Materials Research Bulletin, 1991 , vol. 26, p. 1201 - 1210
in neat (no solvent) byproducts: KCl; mixt. heating at 10 K/min in Ar up 600°C; monitoring by reflected light intensity;
参考文献
Beardell, A. J.; Kirshenbaum, A. D.
Thermochimica Acta, 1974 , vol. 8, p. 35 - 44
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Gmelin Handbook: Mo: SVol.B1, 3.5.5.8, page 118 - 121
