74497-02-2合成路线 （共 11739 条）
反应条件
in methanol reflux; evapn. in vac., recrystn. (EtOAc);
参考文献
Schumann, Manfred; Holtum, Angela von; Wannowius, Klaus J.; Elias, Horst
Inorganic Chemistry, 1982 , vol. 21, p. 606 - 612
反应条件
potassium carbonate; potassium hydrogencarbonate; tetrabutylammomium bromide in tetrachloromethane T=15 - 20°C; 4 h;
参考文献
Zwierzak, Andrzej; Osowska, Krystyna
Synthesis, 1984 , # 3 p. 223 - 224
反应条件
triethylamine in benzene 96 h; Ambient temperature;
参考文献
Moody, Christopher J.; Rees, Charles W.; Thomas, Robert
Tetrahedron, 1992 , vol. 48, # 17 p. 3589 - 3602
反应条件
in benzene 0.5 h; Ambient temperaturefurther educts: O,O'-diethylphosphoric trifluoromethane, -imidazolidosulfuric, -4-methylbenzenesulfonic anhydrides;
参考文献
Dabkowski, Wojciech; Michalski, Jan; Skrzypczynski, Zbigniew
Chemische Berichte, 1985 , vol. 118, # 5 p. 1809 - 1824
反应条件
in benzene 1 h; Ambient temperature;
参考文献
Dabkowski, Wojciech; Michalski, Jan; Radziejewski, Czeslaw; Skrypczynski, Zbigniew
Chemische Berichte, 1982 , vol. 115, # 4 p. 1636 - 1643
反应条件
1.1: sodium nitrite; acetic acid / water / 0.17 h / -15 °C 1.2: 0.75 h / 20 °C 2.1: |Sonication View Scheme
参考文献
Riesel, Lothar; Herrmann, Eckhard; Steinbach, Joerg
Phosphorus and Sulfur and the Related Elements, 1983 , vol. 18, p. 253 - 258
反应条件
triethylamine; hexamethyltriaminodibromophosphorane 1.) CH2Cl2, -20 deg C, 2.) CH2Cl2, RT, 2 h; Yield given. Multistep reaction;
参考文献
Zwierzak, Andrzej; Osowska-Pacewicka, Krystyna
Monatshefte fuer Chemie, 1984 , vol. 115, p. 117 - 120
反应条件
tetrachloromethane Yield given;
参考文献
Riesel, Lothar; Herrmann, Eckhard; Steinbach, Joerg
Phosphorus and Sulfur and the Related Elements, 1983 , vol. 18, p. 253 - 258
反应条件
in acetonitrile T=55°C; Kinetics;
参考文献
Barai, Hasi Rani; Adhikary, Keshab Kumar; Lee, Hai Whang
Bulletin of the Korean Chemical Society, 2012 , vol. 33, # 8 p. 2769 - 2772
参考文献
Michalski et al.
Roczniki Chemii, 1959 , vol. 33, p. 1255
