in water heating to 250°C for 12-48 h at O2-pressure of 90-100atm.;;
参考文献
Henglein, F. A.; Teichmann, L.; Stauf
Z. Anorg. Chem., 1930 , vol. 188, p. 141 - 141
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Gmelin Handbook: I: MVol.2, 103, page 469 - 471
in pyridine heating to 100°C;; decanting from residue; precipitation with benzene; washing with benzene, drying in vac.; product contains 55percent (Ipy)IO3, 42percent (Hpy)IO3, and 3percent HIO3, even after purification;;
Normand, C. W. B.; Cumming, A. C.
Journal of the Chemical Society, 1912 , vol. 101, p. 1854
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Gmelin Handbook: I: MVol.2, 103, page 469 - 471
Lamb; Bray; Geldard
Journal of the American Chemical Society, 1920 , vol. 42, p. 1636 - 1636
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Gmelin Handbook: Cl: MVol., 118, page 316 - 318
