反应条件
1: 1-(tert-butoxy-carbonyl)piperidine With N,N,N',N,-tetramethylethylenediamine; sec.-butyllithium in diethyl ether; hexane T=-78°C; 3 h; 2: With C12H26N2O in diethyl ether; hexane T=-78 - -40°C; 1.5 h; 3: N,N-dimethyl-formamide in diethyl ether; hexane T=-78 - 20°C; Resolution of racemate; optical yield given as percent ee;
参考文献
Coldham, Iain; Raimbault, Sophie; Chovatia, Praful T.; Patel, Jignesh J.; Leonori, Daniele; Sheikh, Nadeem S.; Whittaker, David T. E.
Chemical Communications, 2008 , # 35 p. 4174 - 4176
